香料香精化妆品
香料香精化妝品
향료향정화장품
FLAVOUR FRAGRANCE COSMETICS
2014年
4期
7-11
,共5页
假性紫罗兰酮%β-环糊精%超声波法%包合率%结构表征
假性紫囉蘭酮%β-環糊精%超聲波法%包閤率%結構錶徵
가성자라란동%β-배호정%초성파법%포합솔%결구표정
pseu do ionone%β-cyclodextrin%ultrasonic wave method%inclusion rate%structure characterization
利用超声法制备了假性紫罗兰酮β-环糊精包合物。在单因素试验基础上通过正交试验确定了β-环糊精对假性紫罗兰酮包合的最佳工艺条件为：假性紫罗兰酮与β-环糊精质量比1∶4，包合温度40℃，超声时间60 min。在此条件下假性紫罗兰酮β-环糊精包合物的包合率达到83．89％。验证试验表明，该工艺切实可行，重现性好。采用紫外分光光度法、红外光谱法对包合物进行了结构表征。
利用超聲法製備瞭假性紫囉蘭酮β-環糊精包閤物。在單因素試驗基礎上通過正交試驗確定瞭β-環糊精對假性紫囉蘭酮包閤的最佳工藝條件為：假性紫囉蘭酮與β-環糊精質量比1∶4，包閤溫度40℃，超聲時間60 min。在此條件下假性紫囉蘭酮β-環糊精包閤物的包閤率達到83．89％。驗證試驗錶明，該工藝切實可行，重現性好。採用紫外分光光度法、紅外光譜法對包閤物進行瞭結構錶徵。
이용초성법제비료가성자라란동β-배호정포합물。재단인소시험기출상통과정교시험학정료β-배호정대가성자라란동포합적최가공예조건위：가성자라란동여β-배호정질량비1∶4，포합온도40℃，초성시간60 min。재차조건하가성자라란동β-배호정포합물적포합솔체도83．89％。험증시험표명，해공예절실가행，중현성호。채용자외분광광도법、홍외광보법대포합물진행료결구표정。
Pseu do iononeβ-cyclodextrin inclusion complex was prepared by the ultrasonic wave method. The optimum process conditions were determined by the orthogonal experiment based on the single factor experiment as follows:mass ratio of pseudo ionone toβ-cyclodextrin 1/4,the inclusion temperature 40 ℃ ,ultrasound time 60 min. Under this condition,the inclusion rate of pseudo iononeβ-cyclodextrin inclusion complex reached to 83 .89% . The verifying test showed that this process was feasible and had good reproducibility. The structure of the inclusion complex was characterized by ultraviolet spectroscopy method and infrared spectroscopy method.
