颈腰痛杂志
頸腰痛雜誌
경요통잡지
2014年
5期
494-495
,共2页
李慧芬%张学兰%马艳妮%崔伟亮%曹云飞
李慧芬%張學蘭%馬豔妮%崔偉亮%曹雲飛
리혜분%장학란%마염니%최위량%조운비
花蕊石%煅花蕊石%重金属%砷盐
花蕊石%煅花蕊石%重金屬%砷鹽
화예석%단화예석%중금속%신염
ophicalcitum%calcined ophicalcitum%deposit heavy metals%arsenic salts
目的:制定花蕊石和煅花蕊石中重金属及砷盐等有害元素的含量限度,有效控制该药的质量。方法:采用比色法和古蔡氏法分别测定花蕊石和煅花蕊石中重金属、砷盐含量。结果:测得不同产地的10批样品花蕊石和煅花蕊石含重金属少于2μg·g-1,含砷量少于0.5μg·g-1。结论:该测定方法简便、快速、准确,能有效控制花蕊石和煅花蕊石的质量。
目的:製定花蕊石和煅花蕊石中重金屬及砷鹽等有害元素的含量限度,有效控製該藥的質量。方法:採用比色法和古蔡氏法分彆測定花蕊石和煅花蕊石中重金屬、砷鹽含量。結果:測得不同產地的10批樣品花蕊石和煅花蕊石含重金屬少于2μg·g-1,含砷量少于0.5μg·g-1。結論:該測定方法簡便、快速、準確,能有效控製花蕊石和煅花蕊石的質量。
목적:제정화예석화단화예석중중금속급신염등유해원소적함량한도,유효공제해약적질량。방법:채용비색법화고채씨법분별측정화예석화단화예석중중금속、신염함량。결과:측득불동산지적10비양품화예석화단화예석함중금속소우2μg·g-1,함신량소우0.5μg·g-1。결론:해측정방법간편、쾌속、준학,능유효공제화예석화단화예석적질량。
Objective:Establish the check method of deposit heavy metals and arsenic salts in ophicalcitum and calcined ophicalcitum. Methods:Deposit heavy metals and arsenic salts in ophicalcitum and calcined ophicalcitum were detected by colorimetric method and Gu-Cai method. Results:The content determination of deposit heavy metals in 10 batches of ophicalcitum and calcined ophicalcitum from different origins was less than 2 μg·g-1. The content determination of arsenic salts was less than 0.5 μg·g-1. Conclusion:The method is simple,accurate and can be used to control the quality of ophicalcitum and calcined ophicalci-tum.