测试科学与仪器
測試科學與儀器
측시과학여의기
JOURNAL OF MEASUREMENT SCIENCE AND INSTRUMENTATION
2014年
3期
79-82
,共4页
宗营%姜旭峰%孙静%校云鹏
宗營%薑旭峰%孫靜%校雲鵬
종영%강욱봉%손정%교운붕
中红外光谱%航空润滑油%运动粘度
中紅外光譜%航空潤滑油%運動粘度
중홍외광보%항공윤활유%운동점도
mid-infrared spectrum%aviation lubricating oil%kinematic viscosity
对11个不同基础油含量的50-1-4Ф润滑油样品(标准油)和从现场采集的28个在用50-1-4Φ润滑油样品(在用油)进行傅立叶变换中红外光谱分析。选择1465 cm-1作为测定其运动粘度的特征峰,分别对标准油和在用油样品的运动粘度和相应红外光谱的特征峰处的吸光度进行了相关性分析,给出了回归方程。用另外20个新油样品较正了标准油的回归方程。结果表明,利用傅立叶变换中红外光谱法测定未用及在用50-1-4Φ润滑油的运动粘度是可行的,测定结果是可靠的。
對11箇不同基礎油含量的50-1-4Ф潤滑油樣品(標準油)和從現場採集的28箇在用50-1-4Φ潤滑油樣品(在用油)進行傅立葉變換中紅外光譜分析。選擇1465 cm-1作為測定其運動粘度的特徵峰,分彆對標準油和在用油樣品的運動粘度和相應紅外光譜的特徵峰處的吸光度進行瞭相關性分析,給齣瞭迴歸方程。用另外20箇新油樣品較正瞭標準油的迴歸方程。結果錶明,利用傅立葉變換中紅外光譜法測定未用及在用50-1-4Φ潤滑油的運動粘度是可行的,測定結果是可靠的。
대11개불동기출유함량적50-1-4Ф윤활유양품(표준유)화종현장채집적28개재용50-1-4Φ윤활유양품(재용유)진행부립협변환중홍외광보분석。선택1465 cm-1작위측정기운동점도적특정봉,분별대표준유화재용유양품적운동점도화상응홍외광보적특정봉처적흡광도진행료상관성분석,급출료회귀방정。용령외20개신유양품교정료표준유적회귀방정。결과표명,이용부립협변환중홍외광보법측정미용급재용50-1-4Φ윤활유적운동점도시가행적,측정결과시가고적。
This paper analyzed 11 lubricating oil 50-1-4Φsamples of different base oil content (standar d oil) and 28 used oil samples by Fourier transform mid-infrared spectrometer (FTIR) .First ,the absorption peak of 1 465 cm-1 was selected as the characteristic peak for determining their kinematic viscosities .And then correlation of the kinematic viscosity and the absorbance at characteristic peaks of corresponding infrared spectrum of standard oil and used oil samples was analyzed ,re-spectively ,and two regression equations were proposed . Finally , the regression equation of standard oil was corrected through other 20 new oil samples .The results show that determining kinematic viscosity of new lubricating oil 50-1-4Φ and the used one by FTIR is feasible and reliable .