CAJ | 학술논문

目的：建立冰片中龙脑含量测定的方法，比较不同来源批号的冰片质量。方法：采用气相色谱法，用石英毛细管色谱柱（30m ×0．53mm ×0．6μm）进行检测，最终柱温：200℃。结果：对所采用的测定方法进行了线性回归考察，计算回归方程为：Y ＝0．286X -0．0215， r ＝0．9996；样品在0．28～1．42 mg／mL范围内具有良好的线性关系。结论：经精密度试验，稳定性试验和回收率试验，并经样品含量的测定，表明该检测方法重现性好，准确可靠，可为含冰片的复方制剂的质量控制提供参考方法。
목적：건립빙편중용뇌함량측정적방법，비교불동래원비호적빙편질량。방법：채용기상색보법，용석영모세관색보주（30m ×0．53mm ×0．6μm）진행검측，최종주온：200℃。결과：대소채용적측정방법진행료선성회귀고찰，계산회귀방정위：Y ＝0．286X -0．0215， r ＝0．9996；양품재0．28～1．42 mg／mL범위내구유량호적선성관계。결론：경정밀도시험，은정성시험화회수솔시험，병경양품함량적측정，표명해검측방법중현성호，준학가고，가위함빙편적복방제제적질량공제제공삼고방법。
Objective:To analyze the amount of volatile content in borneol.Methods:Gas chromatography assay was used with capillary column(30m ×0.53mm ×0.6μm), nitrogen as carrier, column temperature:200℃.Results: Linear re-gression examination was used for assay, linear regression equation:Y=0.286X-0.0215(r=0.999 6),it indicated a good linear relationship when borneol was in the range of 0.28~1.42mg/mL.Conclusion:After accuracy test, stability test and retrieve rate test, and assay for the amount in the test sample it indicates that the method applied is good in re-peatability.It may provide a reference method for borneol quality control.