解放军医药杂志
解放軍醫藥雜誌
해방군의약잡지
MEDICAL&PHARMACEUTICAL JOURNAL OF CHINESE PEOPLE'S LIBERATION ARMY
2014年
10期
86-89
,共4页
吴金华%马慧萍%王宁%马骏%何晓英%李兰茹%贾正平
吳金華%馬慧萍%王寧%馬駿%何曉英%李蘭茹%賈正平
오금화%마혜평%왕저%마준%하효영%리란여%가정평
大苞雪莲%黄酮类化合物%正交试验
大苞雪蓮%黃酮類化閤物%正交試驗
대포설련%황동류화합물%정교시험
Saussurea involucrate%Flavonoids%Orthogonal experiment
目的:优选大苞雪莲总黄酮的提取工艺。方法采用L9(34)正交试验,以浸膏得率和雪莲总黄酮含量为指标,考察提取溶剂浓度、溶剂用量、提取时间和提取次数4个因素对提取效果的影响,优选工艺条件。结果最佳提取工艺为10倍量70%乙醇、提取2次,每次2 h,总黄酮含量为12.53%,芦丁含量为2.46%,出膏率为18.20%。结论该提取工艺具有稳定性好和简便易行的优点,适合工业化大生产。
目的:優選大苞雪蓮總黃酮的提取工藝。方法採用L9(34)正交試驗,以浸膏得率和雪蓮總黃酮含量為指標,攷察提取溶劑濃度、溶劑用量、提取時間和提取次數4箇因素對提取效果的影響,優選工藝條件。結果最佳提取工藝為10倍量70%乙醇、提取2次,每次2 h,總黃酮含量為12.53%,蘆丁含量為2.46%,齣膏率為18.20%。結論該提取工藝具有穩定性好和簡便易行的優點,適閤工業化大生產。
목적:우선대포설련총황동적제취공예。방법채용L9(34)정교시험,이침고득솔화설련총황동함량위지표,고찰제취용제농도、용제용량、제취시간화제취차수4개인소대제취효과적영향,우선공예조건。결과최가제취공예위10배량70%을순、제취2차,매차2 h,총황동함량위12.53%,호정함량위2.46%,출고솔위18.20%。결론해제취공예구유은정성호화간편역행적우점,괄합공업화대생산。
Objective To optimize the extraction technology of total flavonoids from Saussurea involucrate. Methods The extraction conditions were optimized by considering the effects of solvent concentration, solvent quantity, extraction time and extraction frequency on extraction, and basing the indexes of the dry extraction rate and content of to-tal flavonoids using L9 ( 34 ) orthogonal design. Results Optimum extracting condition was that 10 times of 70% ethanol was added and extracted for twice with 2 h/each time;total flavonoids content was 12. 53%;Rutin content was 2. 46%;dry extraction rate was 18. 20%. Conclusion The optimized technology is stable, convenient and practical, and it may suit the mass production of Saussurea involucrate.