天津科技
天津科技
천진과기
TIANJIN SCIENCE & TECHNOLOGY
2014年
10期
38-41
,共4页
杨威%王丽敏%唐俊峰%黄晨
楊威%王麗敏%唐俊峰%黃晨
양위%왕려민%당준봉%황신
淀粉%丙烯酰胺%AMPS%降滤失剂
澱粉%丙烯酰胺%AMPS%降濾失劑
정분%병희선알%AMPS%강려실제
starch%acrylamide%AMPS%fluid loss additive
以玉米淀粉(CS)为基体,连续接枝丙烯酰胺(AM)、2-丙烯酰胺基-2-甲基丙磺酸(AMPS)两种单体,合成了 CS/AM、CS/AM/AMPS 两种降滤失剂,并分别对其降滤失性能进行考察。研究结果发现,在 CS 和 AM 的聚合反应中,当反应温度为50,℃,引发剂浓度为单体质量的1.0%,CS与AM的质量比为1∶2,反应时间为3,h时,获得的降滤失剂效果最佳,滤失量为8.6,mL。在此基础上,引入 AMPS,通过正交试验,得出钻井液老化后的最佳反应条件。
以玉米澱粉(CS)為基體,連續接枝丙烯酰胺(AM)、2-丙烯酰胺基-2-甲基丙磺痠(AMPS)兩種單體,閤成瞭 CS/AM、CS/AM/AMPS 兩種降濾失劑,併分彆對其降濾失性能進行攷察。研究結果髮現,在 CS 和 AM 的聚閤反應中,噹反應溫度為50,℃,引髮劑濃度為單體質量的1.0%,CS與AM的質量比為1∶2,反應時間為3,h時,穫得的降濾失劑效果最佳,濾失量為8.6,mL。在此基礎上,引入 AMPS,通過正交試驗,得齣鑽井液老化後的最佳反應條件。
이옥미정분(CS)위기체,련속접지병희선알(AM)、2-병희선알기-2-갑기병광산(AMPS)량충단체,합성료 CS/AM、CS/AM/AMPS 량충강려실제,병분별대기강려실성능진행고찰。연구결과발현,재 CS 화 AM 적취합반응중,당반응온도위50,℃,인발제농도위단체질량적1.0%,CS여AM적질량비위1∶2,반응시간위3,h시,획득적강려실제효과최가,려실량위8.6,mL。재차기출상,인입 AMPS,통과정교시험,득출찬정액노화후적최가반응조건。
In this paper,two kinds of corn starch-based filtrate reducers,CS/AM and CS/AM/AMPS,were synthe-sized through grafting of acrylamide and AMPS continuously and then studied in respect of their filter loss properties. The results indicated that optimum reaction conditions of polymerization of corn starch and acrylamide included a reaction temperature of 50,℃,a monomer initiator quality of 1.0%,a mass ratio of starch and acrylamide of 1∶2, and a reaction time of 3,h. Under such conditions,the filter loss was 8.6,mL. On this basis,AMPS was introduced into the copolymer of CS/AM. Through an orthogonal test,the optimum synthesis condition was obtained.