西部中医药
西部中醫藥
서부중의약
GANSU JOURNAL OF TRADITIONAL CHINESE MEDICINE
2014年
10期
26-27,28
,共3页
黄连解毒合剂%黄芩苷%高效液相色谱法%正交实验
黃連解毒閤劑%黃芩苷%高效液相色譜法%正交實驗
황련해독합제%황금감%고효액상색보법%정교실험
HuanLian JieDu mixture%baicalin%HPLC%orthogonal test
目的：优选黄连解毒合剂提取工艺的最佳条件。方法：以干膏、黄芩苷为评价指标，用正交实验法对黄连解毒合剂进行制备工艺的筛选。结果：最佳提取工艺为煎煮2次，每次加水8倍，第1次1小时，第2次0.5小时，醇沉浓度为55%。结论：该优选工艺合理可行。
目的：優選黃連解毒閤劑提取工藝的最佳條件。方法：以榦膏、黃芩苷為評價指標，用正交實驗法對黃連解毒閤劑進行製備工藝的篩選。結果：最佳提取工藝為煎煮2次，每次加水8倍，第1次1小時，第2次0.5小時，醇沉濃度為55%。結論：該優選工藝閤理可行。
목적：우선황련해독합제제취공예적최가조건。방법：이간고、황금감위평개지표，용정교실험법대황련해독합제진행제비공예적사선。결과：최가제취공예위전자2차，매차가수8배，제1차1소시，제2차0.5소시，순침농도위55%。결론：해우선공예합리가행。
Objective: To optimize the best conditions of extraction process of HuanLian JieDu mixture. Methods:The preparation of HuanLian JieDu mixture was screened by orthogonal test by taking the extract yield and baicalin as the evaluating indexes. Results:The best extraction process was as follows:extracting twice, adding water of eight times, extracting for one hour at the first time, half of one hour at the second time, alcohol-precipitation concentration was 55%. Conclusion:The optimized technology is reasonable and feasible.
