世界中医药
世界中醫藥
세계중의약
WORLD CHINESE MEDICINE
2014年
10期
1361-1363,1366
,共4页
邓义德%易跃能%徐月灿%陈锋%肖满意%刘湘荣
鄧義德%易躍能%徐月燦%陳鋒%肖滿意%劉湘榮
산의덕%역약능%서월찬%진봉%초만의%류상영
白藜芦醇%虎杖%大孔吸附树脂%碱
白藜蘆醇%虎杖%大孔吸附樹脂%堿
백려호순%호장%대공흡부수지%감
Resveratrol%Cuspidatum%Macroporous resin%Alkali
目的:研究大孔吸附树脂分离纯化虎杖中白藜芦醇的工艺条件及参数。方法:利用白藜芦醇显酸性的特点,采用碱液洗脱树脂法分离纯化白藜芦醇。考察6种树脂、碱的浓度以及洗脱流速等因素对白藜芦醇分离纯化的影响。结果:选择NKA-Ⅱ树脂,NaOH洗脱液浓度0.5%,流速为1 BV/h,经过去盐后,白藜芦醇纯度达到70%以上。结论:该工艺适用于对白藜芦醇有吸附的树脂,经过一次上柱就可以与原料中其他干扰成分分离,适合大规模生产。
目的:研究大孔吸附樹脂分離純化虎杖中白藜蘆醇的工藝條件及參數。方法:利用白藜蘆醇顯痠性的特點,採用堿液洗脫樹脂法分離純化白藜蘆醇。攷察6種樹脂、堿的濃度以及洗脫流速等因素對白藜蘆醇分離純化的影響。結果:選擇NKA-Ⅱ樹脂,NaOH洗脫液濃度0.5%,流速為1 BV/h,經過去鹽後,白藜蘆醇純度達到70%以上。結論:該工藝適用于對白藜蘆醇有吸附的樹脂,經過一次上柱就可以與原料中其他榦擾成分分離,適閤大規模生產。
목적:연구대공흡부수지분리순화호장중백려호순적공예조건급삼수。방법:이용백려호순현산성적특점,채용감액세탈수지법분리순화백려호순。고찰6충수지、감적농도이급세탈류속등인소대백려호순분리순화적영향。결과:선택NKA-Ⅱ수지,NaOH세탈액농도0.5%,류속위1 BV/h,경과거염후,백려호순순도체도70%이상。결론:해공예괄용우대백려호순유흡부적수지,경과일차상주취가이여원료중기타간우성분분리,괄합대규모생산。
Objective:To explore purification techniques of Resveratrol by macroporous adsorption resin.Methods:As resveratrol is a-cidic, lye elution resin separation and purification was used.The impact of resin types, NaOH concentration, flow rate on purification results were explored.Results:The optimized purification techniques was: NKA-Ⅱ resin, eluent concentration of NaOH 0.5%, flow rate=1BV/h, after desalting, resveratrol purity >=70%.Conclusion:The optimized purification techniques is applicable to adsorp-tion resin that is resveratrol adsopting, separation with other ingredients can be achieved by one flow, it is suitable for mass production.