世界中医药
世界中醫藥
세계중의약
WORLD CHINESE MEDICINE
2014年
10期
1355-1357
,共3页
川贝止咳合剂%薄层色谱法%高效液相色谱法%质量标准%柚皮苷
川貝止咳閤劑%薄層色譜法%高效液相色譜法%質量標準%柚皮苷
천패지해합제%박층색보법%고효액상색보법%질량표준%유피감
Chuanbeizhike Mixture%TLC%HPLC%Quality standard%Naringin
目的：建立川贝止咳合剂的质量标准控制方法。方法：采用薄层色谱（ TLC）法对方中所含枳壳、桔梗进行定性鉴别；采用高效液相色谱法测定方中柚皮苷的含量。结果：薄层色谱法可鉴别出枳壳、桔梗，且阴性无干扰；柚皮苷在160～800 ng范围内呈良好线性关系，r＝0．9999，平均回收率为98．90％，RSD＝1．32％。结论：本方法操作简便、准确可靠、重现性好，可作为川贝止咳合剂的质量控制方法。
目的：建立川貝止咳閤劑的質量標準控製方法。方法：採用薄層色譜（ TLC）法對方中所含枳殼、桔梗進行定性鑒彆；採用高效液相色譜法測定方中柚皮苷的含量。結果：薄層色譜法可鑒彆齣枳殼、桔梗，且陰性無榦擾；柚皮苷在160～800 ng範圍內呈良好線性關繫，r＝0．9999，平均迴收率為98．90％，RSD＝1．32％。結論：本方法操作簡便、準確可靠、重現性好，可作為川貝止咳閤劑的質量控製方法。
목적：건립천패지해합제적질량표준공제방법。방법：채용박층색보（ TLC）법대방중소함지각、길경진행정성감별；채용고효액상색보법측정방중유피감적함량。결과：박층색보법가감별출지각、길경，차음성무간우；유피감재160～800 ng범위내정량호선성관계，r＝0．9999，평균회수솔위98．90％，RSD＝1．32％。결론：본방법조작간편、준학가고、중현성호，가작위천패지해합제적질량공제방법。
Objective:To establish the quality standard of Chuanbeizhike mixture.Methods:Thin layer chromatography ( TLC) was used to identify Fructus Aurantii, Radix Platycodonis in Chuanbeizhike Mixture.Naringin in Fructus Aurantii was determined by high per-formance liquid chromatography ( HPLC) .Results:The TLC spots of Fructus Aurantii and Radix Platycodonis were clear with good reso-lution and free of interference of negative samples.The calibration curve of HPLC was linear in the range of 160~800ng (r=0.999 9). The average recovery rate was 98.90%, RSD=1.32%.Conclusion:The method is rapid, curate, sensitive and reliable, and it can be used to control the quality of Chuanbeizhike Mixture.
