CAJ | 학술논문

研究自制离子富集脉冲电源对飞行时间质谱仪灵敏度的提高效果。离子富集脉冲电源包括脉冲信号产生模块、放大隔离模块、开关驱动模块、高压电路模块和负载阻抗匹配模块，输出一路中压脉冲信号，两路对称高压脉冲信号。利用自制电喷雾电离源及激光解析电离源与飞行时间质谱仪联用，调试中压脉冲信号。结果显示，应用离子富集脉冲电源后仪器对不同样品的检测灵敏度可提高6~24倍。
연구자제리자부집맥충전원대비행시간질보의령민도적제고효과。리자부집맥충전원포괄맥충신호산생모괴、방대격리모괴、개관구동모괴、고압전로모괴화부재조항필배모괴，수출일로중압맥충신호，량로대칭고압맥충신호。이용자제전분무전리원급격광해석전리원여비행시간질보의련용，조시중압맥충신호。결과현시，응용리자부집맥충전원후의기대불동양품적검측령민도가제고6~24배。
The effect of sensitivity enhancement of time-of-flight mass spectrometer( TOF MS)was studied with home-made ion enrichment pulse power. lon enrichment pulse power includes pulse sig-nal generating module,amplification and isolation module,switching driving module,high voltage circuit module and load impedance matching module,outputing one medium voltage pulse signal and two-way symmetric high voltage pulse signals. ln this work,TOF MS with electrospray ionization ( ESl)was combined with laser desorption ionization( LDl)to debug ion enrichment pulse power. As a conclusion,the detection sensitivity of the instrument could be increased by 6-24 times for differ-ent samples when applying ion enrichment pulse power.