中国中医药信息杂志
中國中醫藥信息雜誌
중국중의약신식잡지
CHINESE JOURNAL OF INFORMATION ON TRADITIONAL CHINESE MEDICINE
2014年
11期
92-94
,共3页
张亚敏%林文津%徐榕青%宋晓瑞%汤权森
張亞敏%林文津%徐榕青%宋曉瑞%湯權森
장아민%림문진%서용청%송효서%탕권삼
泽泻%23-乙酰泽泻醇B%高效液相色谱法%红外光谱%指纹图谱
澤瀉%23-乙酰澤瀉醇B%高效液相色譜法%紅外光譜%指紋圖譜
택사%23-을선택사순B%고효액상색보법%홍외광보%지문도보
Rhizoma Alismatis%23-acetate alisol B%HPLC%infrared spectrometry%fingerprint
目的:比较不同大小泽泻化学成分的差异。方法选取8种不同质量梯度的泽泻药材,采用高效液相色谱法测定其23-乙酰泽泻醇B含量,应用傅里叶变换红外光谱法测定其指纹图谱。结果8种不同质量梯度泽泻中23-乙酰泽泻醇B含量均在0.06%以上,并且其大小与23-乙酰泽泻醇B含量没有相关性(P>0.05),红外指纹图谱相似度均在0.9以上。结论不同大小泽泻的化学成分基本相同,其23-乙酰泽泻醇B含量符合《中华人民共和国药典》规定。
目的:比較不同大小澤瀉化學成分的差異。方法選取8種不同質量梯度的澤瀉藥材,採用高效液相色譜法測定其23-乙酰澤瀉醇B含量,應用傅裏葉變換紅外光譜法測定其指紋圖譜。結果8種不同質量梯度澤瀉中23-乙酰澤瀉醇B含量均在0.06%以上,併且其大小與23-乙酰澤瀉醇B含量沒有相關性(P>0.05),紅外指紋圖譜相似度均在0.9以上。結論不同大小澤瀉的化學成分基本相同,其23-乙酰澤瀉醇B含量符閤《中華人民共和國藥典》規定。
목적:비교불동대소택사화학성분적차이。방법선취8충불동질량제도적택사약재,채용고효액상색보법측정기23-을선택사순B함량,응용부리협변환홍외광보법측정기지문도보。결과8충불동질량제도택사중23-을선택사순B함량균재0.06%이상,병차기대소여23-을선택사순B함량몰유상관성(P>0.05),홍외지문도보상사도균재0.9이상。결론불동대소택사적화학성분기본상동,기23-을선택사순B함량부합《중화인민공화국약전》규정。
Objective To compare the chemical components among Rhizoma Alismatis of different specifications. Methods Rhizoma Alismatis of 8 different weights were chosen, and then contents of 23-acetate alisol B were determined by HPLC, and infrared spectrometry fingerprint was determined by Fourier transform infrared spectroscopy. Results The contents of 23-acetate alisol B in Rhizoma Alismatis of 8 different specifications were over 0.06%, and had no relation with specification of Rhizoma Alismatis (P>0.05). The similarities of infrared spectrometry fingerprint were above 0.9. Conclusion The chemical components among Rhizoma Alismatis of different specifications were basically the same. Contents of 23-acetate alisol B of Rhizoma Alismatis of 8 different specifications conformed to regulation of China Pharmacopoeia.