CAJ | 학술논문

目的：建立爱维心口服液质量标准。方法采用薄层色谱法对制剂中的丁香、西红花进行鉴别,采用气相色谱法测定丁香中丁香酚的含量。结果丁香、西红花的薄层色谱特征斑点分离清晰,阴性对照无干扰。丁香酚在0.05217～2.0868μg范围内线性关系良好(r＝0.9999),供试品溶液在24 h内稳定,平均加样回收率为95.7%,RSD＝1.4%(n＝6)。结论本方法简单、准确可靠、重复性好,可用于控制爱维心口服液的质量。
목적：건립애유심구복액질량표준。방법채용박층색보법대제제중적정향、서홍화진행감별,채용기상색보법측정정향중정향분적함량。결과정향、서홍화적박층색보특정반점분리청석,음성대조무간우。정향분재0.05217～2.0868μg범위내선성관계량호(r＝0.9999),공시품용액재24 h내은정,평균가양회수솔위95.7%,RSD＝1.4%(n＝6)。결론본방법간단、준학가고、중복성호,가용우공제애유심구복액적질량。
Objective To establish a quality standard for Aiweixin oral liquid. Methods TLC was applied to the identification of Caryophylli Flos and Crocin in Aiweixin oral liquid. Eugenol was analyzed by GC. Results TLC of Caryophylli Flos and Crocin had distinct separation of characteristic spots and there was no interference in negative comparison. The linear response ranges of Eugenol were between 0.052 17-2.086 8μg (r=0.999 9). The samples were steady within 24 h. The average recovery of eugenol was 95.7%, RSD=1.4% (n=6). Conclusion The method is simple, accurate and reliable, and can be used for the quality control of Aiweixin oral liquid.