哈尔滨商业大学学报(自然科学版)
哈爾濱商業大學學報(自然科學版)
합이빈상업대학학보(자연과학판)
JOURNAL OF HARBIN UNIVERSITY OF COMMERCE(NATURAL SCIENCES EDITION)
2014年
5期
558-560,576
,共4页
东方%于蕾%程斌%郭守东%王翀%余玥%冮剑
東方%于蕾%程斌%郭守東%王翀%餘玥%冮劍
동방%우뢰%정빈%곽수동%왕충%여모%강검
刺山柑%刺山柑多糖%表征结构
刺山柑%刺山柑多糖%錶徵結構
자산감%자산감다당%표정결구
Cappraris spinosa L .%CSPSI-C%characterization
刺山柑多糖为刺山柑中主要成分,对其表征结构进行研究十分必要。采用扫描电子显微镜、粒径电荷分析仪、差式扫描量热仪、X-射线衍射仪及刚果红实验探讨了CSPSI-C的表征结构。结果表明,CSPSI-C为鳞片状、棒状及枝链状形态。并得到了其粒径和Zeta大小。热力学分析显示了CSPSI-C的热力学特性,X-射线衍射表明CSPSI-C为无定形态,刚果红实验提示CSPSI-C具有多股螺旋结构。研究了CSPSI-C的表征结构,为进一步研究其构效关系奠定基础。
刺山柑多糖為刺山柑中主要成分,對其錶徵結構進行研究十分必要。採用掃描電子顯微鏡、粒徑電荷分析儀、差式掃描量熱儀、X-射線衍射儀及剛果紅實驗探討瞭CSPSI-C的錶徵結構。結果錶明,CSPSI-C為鱗片狀、棒狀及枝鏈狀形態。併得到瞭其粒徑和Zeta大小。熱力學分析顯示瞭CSPSI-C的熱力學特性,X-射線衍射錶明CSPSI-C為無定形態,剛果紅實驗提示CSPSI-C具有多股螺鏇結構。研究瞭CSPSI-C的錶徵結構,為進一步研究其構效關繫奠定基礎。
자산감다당위자산감중주요성분,대기표정결구진행연구십분필요。채용소묘전자현미경、립경전하분석의、차식소묘량열의、X-사선연사의급강과홍실험탐토료CSPSI-C적표정결구。결과표명,CSPSI-C위린편상、봉상급지련상형태。병득도료기립경화Zeta대소。열역학분석현시료CSPSI-C적열역학특성,X-사선연사표명CSPSI-C위무정형태,강과홍실험제시CSPSI-C구유다고라선결구。연구료CSPSI-C적표정결구,위진일보연구기구효관계전정기출。
As the main component of Cappraris spinosa L ., it is necessary to investigate the Cappraris spinosa L .polysaccharide characterization .This paper explored the structure of CSPSI-C by the scanning electron microscope , nano-particle size and zeta potential analy-zer, differential scanning calorimetry , X-ray diffraction and Congo red experiments .Under the scanning electron microscope , the morphology of CSPSI -C presented long strip and rod . Particles size and Zeta were also obtained .Thermodynamic analysis showed that the thermo-dynamic characteristics of CSPSI -C.X-ray diffraction showed that CSPSI -C was amor-phous and congo red experiments suggested that CSPSI -C had helix structure .This paper explored the characterization of CSPSI -C to establish the foundation for the structure -ac-tivity relationship .