食品研究与开发
食品研究與開髮
식품연구여개발
FOOD RESEARCH AND CEVELOPMENT
2014年
18期
55-58
,共4页
肖亚兵%何健%崔颖
肖亞兵%何健%崔穎
초아병%하건%최영
Chelex-100%螯合树脂%铜%海水
Chelex-100%螯閤樹脂%銅%海水
Chelex-100%오합수지%동%해수
Chelex-100%chelating resin%copper%seawater
对Chelex-100树脂对铜和钠的吸附系数Kd进行了测定，研究pH对吸附效果的影响，分析铜和钠的柱行为，并绘制了淋洗曲线，测定Chelex-100树脂对铅、镉、铜的吸附容量。使用自制小型离子交换柱，建立Chelex-100树脂分离-石墨炉原子吸收法测定养殖用海水中铜的方法，成功将铜与氯化钠基体分离，消除了基体干扰。方法回收率：94%～102%， RSD：1.5%～4.2%。
對Chelex-100樹脂對銅和鈉的吸附繫數Kd進行瞭測定，研究pH對吸附效果的影響，分析銅和鈉的柱行為，併繪製瞭淋洗麯線，測定Chelex-100樹脂對鉛、鎘、銅的吸附容量。使用自製小型離子交換柱，建立Chelex-100樹脂分離-石墨爐原子吸收法測定養殖用海水中銅的方法，成功將銅與氯化鈉基體分離，消除瞭基體榦擾。方法迴收率：94%～102%， RSD：1.5%～4.2%。
대Chelex-100수지대동화납적흡부계수Kd진행료측정，연구pH대흡부효과적영향，분석동화납적주행위，병회제료림세곡선，측정Chelex-100수지대연、력、동적흡부용량。사용자제소형리자교환주，건립Chelex-100수지분리-석묵로원자흡수법측정양식용해수중동적방법，성공장동여록화납기체분리，소제료기체간우。방법회수솔：94%～102%， RSD：1.5%～4.2%。
Separation method using Chelex-100 chelating resin and GFAAS determination of copper in seawater for culture was eatablished. This method could solve the problem of interference on the determination of copper from sodium chloride matrix. Kd value of Na and Cu on chelating resin was detected. The influence of pH value of solution on adsorption and behavior of ion on resin were analyzed. Elution curve for Na and Cu was drawn. Adsorption capacity of resin was detected. Recovery of method:94%-102%, RSD:1.5%-4.2%.
