耐火材料
耐火材料
내화재료
REFRACTORIES
2014年
5期
356-358,364
,共4页
多孔莫来石%木炭%添加量%常温耐压强度%显气孔率
多孔莫來石%木炭%添加量%常溫耐壓彊度%顯氣孔率
다공막래석%목탄%첨가량%상온내압강도%현기공솔
porous mullite%charcoal%addition%cold crushing strength%apparent porosity
为了改善以木炭为造孔剂的多孔莫来石陶瓷的性能,以烧结莫来石(0.25~0.3 mm)、SiO2微粉、Al2 O3微粉、滑石粉、球黏土、膨润土、甲基纤维素、木炭粉(≤0.044 mm)为原料,研究了不同量的木炭粉(外加质量分数分别为0、2%、4%、6%、8%、10%、12%)对多孔莫来石坯体的成型外观、烘干后的常温耐压强度及1400℃保温3h热处理后的显气孔率和常温耐压强度的影响,并对不同木炭添加量的多孔莫来石试样进行了显微结构分析。结果表明:外加质量分数≤8%的木炭,制成的多孔莫来石坯体可较好成型;外加质量分数2%~8%木炭的莫来石坯体与不添加木炭的相比,烘干后试样的常温耐压强度明显提高;多孔莫来石热处理后的显气孔率随着木炭添加量的增加而增加,常温耐压强度随之降低。综合考虑多孔莫来石陶瓷各项性能,木炭外加质量分数不宜超过8%。
為瞭改善以木炭為造孔劑的多孔莫來石陶瓷的性能,以燒結莫來石(0.25~0.3 mm)、SiO2微粉、Al2 O3微粉、滑石粉、毬黏土、膨潤土、甲基纖維素、木炭粉(≤0.044 mm)為原料,研究瞭不同量的木炭粉(外加質量分數分彆為0、2%、4%、6%、8%、10%、12%)對多孔莫來石坯體的成型外觀、烘榦後的常溫耐壓彊度及1400℃保溫3h熱處理後的顯氣孔率和常溫耐壓彊度的影響,併對不同木炭添加量的多孔莫來石試樣進行瞭顯微結構分析。結果錶明:外加質量分數≤8%的木炭,製成的多孔莫來石坯體可較好成型;外加質量分數2%~8%木炭的莫來石坯體與不添加木炭的相比,烘榦後試樣的常溫耐壓彊度明顯提高;多孔莫來石熱處理後的顯氣孔率隨著木炭添加量的增加而增加,常溫耐壓彊度隨之降低。綜閤攷慮多孔莫來石陶瓷各項性能,木炭外加質量分數不宜超過8%。
위료개선이목탄위조공제적다공막래석도자적성능,이소결막래석(0.25~0.3 mm)、SiO2미분、Al2 O3미분、활석분、구점토、팽윤토、갑기섬유소、목탄분(≤0.044 mm)위원료,연구료불동량적목탄분(외가질량분수분별위0、2%、4%、6%、8%、10%、12%)대다공막래석배체적성형외관、홍간후적상온내압강도급1400℃보온3h열처리후적현기공솔화상온내압강도적영향,병대불동목탄첨가량적다공막래석시양진행료현미결구분석。결과표명:외가질량분수≤8%적목탄,제성적다공막래석배체가교호성형;외가질량분수2%~8%목탄적막래석배체여불첨가목탄적상비,홍간후시양적상온내압강도명현제고;다공막래석열처리후적현기공솔수착목탄첨가량적증가이증가,상온내압강도수지강저。종합고필다공막래석도자각항성능,목탄외가질량분수불의초과8%。
Sintered mullite(0.25 -0.3 mm),SiO2 micropowder,Al2 O3 micropowder,talc powder,ball clay, amargosite,methylcellulose and charcoal powder(≤0.044 mm)were used as main starting materials to im-prove the properties of porous mullite ceramics with charcoal powder as the pore former.The influences of charcoal powder addition (extra-added 0,2%,4%,6%,8%,10%and 12%,respectively,in mass,the same hereinafter)on moldability of green bodies,CCS of dried specimens,CCS and AP of specimens treated at 1 400 ℃for 3 h were studied,and the microstructure of porous mullite specimens was analyzed.The results show that:the mullite green bodies with ≤8% charcoal powder has good moldability;compared with the specimens without charcoal powder,CCS of the dried specimens with 2%-8%charcoal powder improves obviously;with the charcoal powder increasing,the AP of the heat-treated specimens increases and CCS decreases.Thus,the appropriate charcoal addition in porous mullite ceramics shall not be more than 8%.