世界中医药
世界中醫藥
세계중의약
WORLD CHINESE MEDICINE
2014年
9期
1228-1230
,共3页
木蝴蝶%黄芩苷%薄层层析%质量标准
木蝴蝶%黃芩苷%薄層層析%質量標準
목호접%황금감%박층층석%질량표준
Semen oroxyli%Baicalin%TLC%Quality standards
目的：研究木蝴蝶药材的质量标准。方法：性状鉴定，粉末显微鉴定，以黄芩苷对照品作对照进行 TLC 鉴别，按《中华人民共和国药典》2010年版（一部）要求对其中的水分、总灰分、酸不溶灰分、杂质、醇溶性浸出物等指标进行分析。结果：市售5批药材中水分、醇溶性浸出物含量均符合药典标准，醇溶性浸出物含量以云南最高，达31.09％。确定了木蝴蝶药材总灰分范围：3.16％～3.99％；酸不溶灰分范围：0.01％～0.06％；杂质含量范围：0.04％～0.09％，并对其含量限度提出了建议。结论：研究结果为进一步完善木蝴蝶药材质量标准提供依据。
目的：研究木蝴蝶藥材的質量標準。方法：性狀鑒定，粉末顯微鑒定，以黃芩苷對照品作對照進行 TLC 鑒彆，按《中華人民共和國藥典》2010年版（一部）要求對其中的水分、總灰分、痠不溶灰分、雜質、醇溶性浸齣物等指標進行分析。結果：市售5批藥材中水分、醇溶性浸齣物含量均符閤藥典標準，醇溶性浸齣物含量以雲南最高，達31.09％。確定瞭木蝴蝶藥材總灰分範圍：3.16％～3.99％；痠不溶灰分範圍：0.01％～0.06％；雜質含量範圍：0.04％～0.09％，併對其含量限度提齣瞭建議。結論：研究結果為進一步完善木蝴蝶藥材質量標準提供依據。
목적：연구목호접약재적질량표준。방법：성상감정，분말현미감정，이황금감대조품작대조진행 TLC 감별，안《중화인민공화국약전》2010년판（일부）요구대기중적수분、총회분、산불용회분、잡질、순용성침출물등지표진행분석。결과：시수5비약재중수분、순용성침출물함량균부합약전표준，순용성침출물함량이운남최고，체31.09％。학정료목호접약재총회분범위：3.16％～3.99％；산불용회분범위：0.01％～0.06％；잡질함량범위：0.04％～0.09％，병대기함량한도제출료건의。결론：연구결과위진일보완선목호접약재질량표준제공의거。
Objective:To study the quality standards of Semen oroxyli.Methods:Characteristic identification,microscopic identifica-tion and thin layer chromatography (TLC)were adopted,and baicalin was used as reference control.Analysis was given according to the standards on moisture,total ash,insoluble ash and impurity in acid,alcohol soluble extract in Chinese pharmacopoeia (year 2000 e-dition).Results:The contents of moisture and alcohol-soluble extract of the five bunch of medicine sold in market all complied with the standards of Chinese pharmacopoeia.The Semen oroxyli in Yunnan had the most contents of alcohol-soluble extract,accounting for 31. 09%.The range of contents of total ash,insoluble ash and impurities of the Semen oroxyli were identified to be 3.16% to 3.99%, 0.01% to 0.06%,and 0.04% to 0.09% respectively.Advises on its content limit was proposed.Conclusion:These results can pro-vide references for further studies on the quality standards of Semen oroxyli.
