当代化工
噹代化工
당대화공
CONTEMPORARY CHEMICAL INDUSTRY
2014年
10期
2199-2202
,共4页
太史剑瑶%程仲芊%凌凤香
太史劍瑤%程仲芊%凌鳳香
태사검요%정중천%릉봉향
超临界流体色谱%柴油%芳烃
超臨界流體色譜%柴油%芳烴
초림계류체색보%시유%방경
Supercritical fluid chromatography%Diesel%Aromatic hydrocarbon
采用超临界流体色谱法,测定柴油中单环和多环芳烃的含量。芳烃加标回收实验测定结果的回收率在97.5%~101.6%之间。单环和多环芳烃的重复性实验的测定结果最大偏差不超过0.4个单位。与质谱法分析的数据对比,两种方法的线性相关系数可达到0.99以上。
採用超臨界流體色譜法,測定柴油中單環和多環芳烴的含量。芳烴加標迴收實驗測定結果的迴收率在97.5%~101.6%之間。單環和多環芳烴的重複性實驗的測定結果最大偏差不超過0.4箇單位。與質譜法分析的數據對比,兩種方法的線性相關繫數可達到0.99以上。
채용초림계류체색보법,측정시유중단배화다배방경적함량。방경가표회수실험측정결과적회수솔재97.5%~101.6%지간。단배화다배방경적중복성실험적측정결과최대편차불초과0.4개단위。여질보법분석적수거대비,량충방법적선성상관계수가체도0.99이상。
Supercritical fluid chromatography was used to determine mono-aromatic and polycyclic aromatic hydrocarbons (PAHs) content of diesel. The experiment of aromatic standard recovery rate showedthat the recovery rate result wasbetween 97.5%~101.6%. The maximum deviation of repeatability experiment for mono-aromatic and polycyclic aromatic hydrocarbons (PAHs) was notmore than 0.4 units. Compared with the method of mass spectrometry, the linear correlation coefficient of the two methods could reach above 0.99.