云南中医学院学报
雲南中醫學院學報
운남중의학원학보
JOURNAL OF YUNNAN COLLEGE OF TRADITIONAL CHINESE MEDICINE
2014年
5期
36-38,44
,共4页
王煊镇%盛晓静%刘薇%张晓云
王煊鎮%盛曉靜%劉薇%張曉雲
왕훤진%성효정%류미%장효운
清毒百炎消软膏%质量标准%半边莲%绿原酸
清毒百炎消軟膏%質量標準%半邊蓮%綠原痠
청독백염소연고%질량표준%반변련%록원산
Qingdu Baiyanxiao ointment%quality standard%Lobelia Chinensis Lour%chlorogenic acid
目的:提高清毒百炎消软膏质量标准。方法对处方中半边莲药材进行TLC鉴别,用HPLC测定绿原酸含量。结果薄层色谱斑点清晰,专属性强;绿原酸的含量测定范围在0.07288μg~1.458μg线性关系良好,r=0.9999,平均回收率为99.80%,RSD为0.5%.结论方法简便准确,可用于清毒百炎消软膏的质量控制。
目的:提高清毒百炎消軟膏質量標準。方法對處方中半邊蓮藥材進行TLC鑒彆,用HPLC測定綠原痠含量。結果薄層色譜斑點清晰,專屬性彊;綠原痠的含量測定範圍在0.07288μg~1.458μg線性關繫良好,r=0.9999,平均迴收率為99.80%,RSD為0.5%.結論方法簡便準確,可用于清毒百炎消軟膏的質量控製。
목적:제고청독백염소연고질량표준。방법대처방중반변련약재진행TLC감별,용HPLC측정록원산함량。결과박층색보반점청석,전속성강;록원산적함량측정범위재0.07288μg~1.458μg선성관계량호,r=0.9999,평균회수솔위99.80%,RSD위0.5%.결론방법간편준학,가용우청독백염소연고적질량공제。
Objective To improve the quality standard for Qingdu Baiyanxiao Ointment. Methods Lobelia Chinensis Lour in the prescription was identified by TLC, and the content of chlorogenic acid was determined by HPLC. Results TLC spots were clear, with strong specificity. Chlorogenic acid showed a good linear relationship at the range of 0.07288μg-1.458μg, r=0.9999. The average recovery was 99.80%and RSD was 0.5%. Conclusion The established method is Simple, accurate, and can be used for the quality control of Qingdu Baiyanxiao Ointment.