吉林师范大学学报(自然科学版)
吉林師範大學學報(自然科學版)
길림사범대학학보(자연과학판)
JILIN NORMAL UNIVERSITY JOURNAL(NATURAL SCIENCE EDITION)
2014年
4期
77-79
,共3页
有机物%2-对氟苯甲酰苯胺%单晶 X-射线衍射
有機物%2-對氟苯甲酰苯胺%單晶 X-射線衍射
유궤물%2-대불분갑선분알%단정 X-사선연사
organic matter%2-(4-fluorobenzoyl)aniline%single-crystal x-ray diffraction
在实验条件下合成了有机化合物2-对氟苯甲酰苯胺(C13 H10 NOF),并通过元素分析和单晶 X-射线衍射对其进行了表征.结果表明该化合物属于单斜晶系:空间群 P2(1)/ c,晶胞参数 a =10.4539,b =11.2863,c =9.0041?,β=99.658(5)°,C13 H10 NOF,Mr =215.22,V =1047.30 F(000)=448.0 Mu =0.10 mm-1 Cell Wt=860.88 Rho =1.365.
在實驗條件下閤成瞭有機化閤物2-對氟苯甲酰苯胺(C13 H10 NOF),併通過元素分析和單晶 X-射線衍射對其進行瞭錶徵.結果錶明該化閤物屬于單斜晶繫:空間群 P2(1)/ c,晶胞參數 a =10.4539,b =11.2863,c =9.0041?,β=99.658(5)°,C13 H10 NOF,Mr =215.22,V =1047.30 F(000)=448.0 Mu =0.10 mm-1 Cell Wt=860.88 Rho =1.365.
재실험조건하합성료유궤화합물2-대불분갑선분알(C13 H10 NOF),병통과원소분석화단정 X-사선연사대기진행료표정.결과표명해화합물속우단사정계:공간군 P2(1)/ c,정포삼수 a =10.4539,b =11.2863,c =9.0041?,β=99.658(5)°,C13 H10 NOF,Mr =215.22,V =1047.30 F(000)=448.0 Mu =0.10 mm-1 Cell Wt=860.88 Rho =1.365.
The title compound,2-(4-fluorobenzoyl)aniline(C13 H10 NOF Mr = 215. 22),has been synthesized and characterized by single-crystal X-ray diffraction. The crystal of the title compound belongs to monoclinic,space group P2(1)/ c,a = 10. 453 9,b = 11. 286 3,c = 9. 004 1 ?,β = 99. 658(5)°,C13 H10 NOF,Mr = 215. 22,V =1047. 30 F(000)= 448. 0 Mu = 0. 10 mm - 1 Cell Wt = 860. 88 Rho = 1. 365.