中国药师
中國藥師
중국약사
CHINA PHARMACIST
2014年
11期
1984-1986
,共3页
杨庆懿%罗艳%龙凌云%王伟姣%殷帅%李文莉
楊慶懿%囉豔%龍凌雲%王偉姣%慇帥%李文莉
양경의%라염%룡릉운%왕위교%은수%리문리
山楂%保健食品%展青霉素%高效液相色谱法
山楂%保健食品%展青黴素%高效液相色譜法
산사%보건식품%전청매소%고효액상색보법
Hawthorn%Health food%Patulin%HPLC
目的：建立含山楂类保健食品中展青霉素的含量测定方法,完善相关保健食品中展青霉素的质量控制。方法：色谱柱：Agilent TC-C18(2)柱(250 mm ×4.6 mm,5μm)；流动相：0.8%四氢呋喃溶液；流速：1.0 ml·min-1；柱温：30℃；检测波长：276 nm。结果：展青霉素在1~20 ng范围内线性关系良好(r=1.0000),平均加样回收率为92.1%,RSD=2.2%(n=6)。结论：本法简便、可靠、准确,可用于含山楂类保健食品中展青霉素的含量测定。
目的：建立含山楂類保健食品中展青黴素的含量測定方法,完善相關保健食品中展青黴素的質量控製。方法：色譜柱：Agilent TC-C18(2)柱(250 mm ×4.6 mm,5μm)；流動相：0.8%四氫呋喃溶液；流速：1.0 ml·min-1；柱溫：30℃；檢測波長：276 nm。結果：展青黴素在1~20 ng範圍內線性關繫良好(r=1.0000),平均加樣迴收率為92.1%,RSD=2.2%(n=6)。結論：本法簡便、可靠、準確,可用于含山楂類保健食品中展青黴素的含量測定。
목적：건립함산사류보건식품중전청매소적함량측정방법,완선상관보건식품중전청매소적질량공제。방법：색보주：Agilent TC-C18(2)주(250 mm ×4.6 mm,5μm)；류동상：0.8%사경부남용액；류속：1.0 ml·min-1；주온：30℃；검측파장：276 nm。결과：전청매소재1~20 ng범위내선성관계량호(r=1.0000),평균가양회수솔위92.1%,RSD=2.2%(n=6)。결론：본법간편、가고、준학,가용우함산사류보건식품중전청매소적함량측정。
Objective:To establish an HPLC method for the determination of patulin in health foods containing hawthorn to im-prove the quality control of patulin in related health foods. Methods:An Agilent TC-C18(2)(250 mm ×4.6 mm, 5 μm) column was used with the temperature of 30℃. The mobile phase consisted of 0. 8% tetrahydrofuran and the flow rate was 1. 0 ml·min-1 . The detection wavelength was set at 276nm. Results:The calibration curve of patulin was linear within the range of 1-20ng(r=1. 000 0), the average recovery was 92. 1% and RSD was 2. 2%(n=6). Conclusion:The method is simple, reliable and accurate, which can be used in the content determination of patulin in health foods containing hawthorn.
