中国药师
中國藥師
중국약사
CHINA PHARMACIST
2014年
11期
1830-1832
,共3页
七叶灵颗粒%质量标准%薄层色谱法%高效液相色谱法
七葉靈顆粒%質量標準%薄層色譜法%高效液相色譜法
칠협령과립%질량표준%박층색보법%고효액상색보법
Qiyeling granules%Quality standard%TLC%HPLC
目的：建立七叶灵颗粒的质量标准。方法：采用薄层色谱法对黄芪、柚皮苷进行定性鉴别；采用高效液相色谱法对黄芪甲苷进行含量测定。结果：定性鉴别阴性无干扰,分离度高；黄芪甲苷线性范围为0.166~1.104μg(r=0.9991),平均回收率为97.27%,RSD为1.3%(n=6)。结论：所建标准可以用于七叶灵颗粒的质量控制。
目的：建立七葉靈顆粒的質量標準。方法：採用薄層色譜法對黃芪、柚皮苷進行定性鑒彆；採用高效液相色譜法對黃芪甲苷進行含量測定。結果：定性鑒彆陰性無榦擾,分離度高；黃芪甲苷線性範圍為0.166~1.104μg(r=0.9991),平均迴收率為97.27%,RSD為1.3%(n=6)。結論：所建標準可以用于七葉靈顆粒的質量控製。
목적：건립칠협령과립적질량표준。방법：채용박층색보법대황기、유피감진행정성감별；채용고효액상색보법대황기갑감진행함량측정。결과：정성감별음성무간우,분리도고；황기갑감선성범위위0.166~1.104μg(r=0.9991),평균회수솔위97.27%,RSD위1.3%(n=6)。결론：소건표준가이용우칠협령과립적질량공제。
Objective:To establish the quality standard for Qiyeling granules. Methods:Astragali Radix and naringin were identi-fied by TLC. The content of astragaloside A was determined by HPLC. Results:The qualitative identification was with high resolution and without interference from the negative substances. The linear range of astragaloside A was 0. 166-1. 104 μg(r=0. 999 1), and the average recovery was 97. 27%(RSD=1. 3%,n=6). Conclusion:The method can be used in the quality control of Qiyeling granules.
