甘肃农业大学学报
甘肅農業大學學報
감숙농업대학학보
JOURNAL OF GANSU AGRICULTURAL UNIVERSITY
2014年
5期
164-170,175
,共8页
张志龙%韩舜愈%祝霞%张波%侯晓瑞%陈伦佳
張誌龍%韓舜愈%祝霞%張波%侯曉瑞%陳倫佳
장지룡%한순유%축하%장파%후효서%진륜가
‘黑比诺’葡萄%武威地区%液液萃取%GC-MS%香气成分%OAV
‘黑比諾’葡萄%武威地區%液液萃取%GC-MS%香氣成分%OAV
‘흑비낙’포도%무위지구%액액췌취%GC-MS%향기성분%OAV
‘Pinot Noir’grape%Wuwei region%liquid-liquid extraction%gas chromatography-mass spec-trometry%volatile component%odor activity value
以武威地区凉州区黄羊河农场和民勤苏武山两个葡萄园区葡萄原料酿造的‘黑比诺’干红葡萄酒为试验原料,以二氯甲烷为萃取剂,通过液液萃取法提取葡萄酒香气成分,运用 GC-MS技术对其香气成分进行分析,采用气味活度值(OAV)评价各香气化合物对酒样总体香气的贡献.酒样中共检出57种香气成分,主要香气物质为:3-甲基-1-丁醇、2-甲基丙醇、乙酸乙酯、乙酸、苯乙醇、正丙醇、2,3-丁二醇、正己酸、3-羟基-2-丁酮;主要香气贡献物有:3-甲基-1-丁醇、2-甲基丙醇、苯乙醇、辛酸乙酯、乙酸异戊酯、乙酸乙酯、异戊酸、2-甲基丁酸、己酸和辛酸.其中,黄羊河农场酒样中共检出53种香气成分,香气总量为593.49 mg/L,苏武山酒样中共检出26种香气成分,香气总量为472.62 mg/L.对比分析两个产地的‘黑比诺’干红葡萄酒,其主要香气成分和香气贡献物在种类和含量上均有所差异,赋予葡萄酒不同的香气特性.
以武威地區涼州區黃羊河農場和民勤囌武山兩箇葡萄園區葡萄原料釀造的‘黑比諾’榦紅葡萄酒為試驗原料,以二氯甲烷為萃取劑,通過液液萃取法提取葡萄酒香氣成分,運用 GC-MS技術對其香氣成分進行分析,採用氣味活度值(OAV)評價各香氣化閤物對酒樣總體香氣的貢獻.酒樣中共檢齣57種香氣成分,主要香氣物質為:3-甲基-1-丁醇、2-甲基丙醇、乙痠乙酯、乙痠、苯乙醇、正丙醇、2,3-丁二醇、正己痠、3-羥基-2-丁酮;主要香氣貢獻物有:3-甲基-1-丁醇、2-甲基丙醇、苯乙醇、辛痠乙酯、乙痠異戊酯、乙痠乙酯、異戊痠、2-甲基丁痠、己痠和辛痠.其中,黃羊河農場酒樣中共檢齣53種香氣成分,香氣總量為593.49 mg/L,囌武山酒樣中共檢齣26種香氣成分,香氣總量為472.62 mg/L.對比分析兩箇產地的‘黑比諾’榦紅葡萄酒,其主要香氣成分和香氣貢獻物在種類和含量上均有所差異,賦予葡萄酒不同的香氣特性.
이무위지구량주구황양하농장화민근소무산량개포도완구포도원료양조적‘흑비낙’간홍포도주위시험원료,이이록갑완위췌취제,통과액액췌취법제취포도주향기성분,운용 GC-MS기술대기향기성분진행분석,채용기미활도치(OAV)평개각향기화합물대주양총체향기적공헌.주양중공검출57충향기성분,주요향기물질위:3-갑기-1-정순、2-갑기병순、을산을지、을산、분을순、정병순、2,3-정이순、정기산、3-간기-2-정동;주요향기공헌물유:3-갑기-1-정순、2-갑기병순、분을순、신산을지、을산이무지、을산을지、이무산、2-갑기정산、기산화신산.기중,황양하농장주양중공검출53충향기성분,향기총량위593.49 mg/L,소무산주양중공검출26충향기성분,향기총량위472.62 mg/L.대비분석량개산지적‘흑비낙’간홍포도주,기주요향기성분화향기공헌물재충류화함량상균유소차이,부여포도주불동적향기특성.
The volatile compounds of‘Pinot Noir’dry red wine from two producers (Huangyanghe and Suwushan)in Wuwei were analyzed with dichloromethane as the extracts and gas chromatography-mass spectrometry (GC-MS).The odor activity value (OVA)was employed for evaluating the contribution of volatile compounds.The result showed that 5 7 aroma compounds were identified.The maj or compounds in-cluded 3-methyl-1-butanol,2-methyl-propanol,ethyl acetate,acetic acid,phenyl ethanol,1-propanol,2,3-bu-tanediol,1-hexanoic acid,3-hydroxy-2-butanone.The main contributing compounds included 3-methyl-1-bu-tanol,2-methyl-propanol,benzyl alcohol,ethyl octanoate,isoamyl acetate,ethyl acetate,isovaleric acid,2-methyl-butyric acid,hexanoic acid and octanoate.There were 53 aroma compounds identified form Huangy-anghe wine,26 aroma compounds identified from Suwushan wine,the total aroma content was 593.49 mg/L and 472.62 mg/L respectively.It is suggested that there is a significant difference in type and content of major volatile compounds and main contributing compounds,the differences represent their own specific flavor characteristics.