CAJ | 학술논문

目的：建立全痔膏中冰片、硼砂、滑石粉、朱砂和银朱药味的质量控制方法。方法分别采用薄层色谱法，理化分析法，原子荧光分光光度法。结果冰片薄层鉴别实验重现性良好；硼砂和滑石粉理化反应鉴别试验重现性良好；原子荧光分光光度法测朱砂与银朱中硫化汞含量实验结果符合规定。结论该方法简便易行，准确可靠，可用于全痔膏的质量控制。
목적：건립전치고중빙편、붕사、활석분、주사화은주약미적질량공제방법。방법분별채용박층색보법，이화분석법，원자형광분광광도법。결과빙편박층감별실험중현성량호；붕사화활석분이화반응감별시험중현성량호；원자형광분광광도법측주사여은주중류화홍함량실험결과부합규정。결론해방법간편역행，준학가고，가용우전치고적질량공제。
Objective To establish the quality control method of ingredients borneol, borax, talcum powder, cinnabar and vermillion cinnabar in Quan Zhi Gao. Methods The thin layer chromatography (TLC), the physical and chemical analysis method and atomic fluorescence spec-trophotometry were used in the analyses, respectively. Results The identifying TLC experiments of borneol and physical and chemical analysis identifying experiments of borax and talcum powder, all have good reproducibilities. HgS contents in cinnabar and vermilion conformed to the provisions. Conclusion The method established is simple, accurate, reliable and can be used in quality control of Quan Zhi Gao.