CAJ | 학술논문

本文建立了策划药物亚甲基二氧吡咯戊酮（MDPV）的气相色谱-质谱（GC-MS）联用、液相色谱-质谱（LC-MS）联用分析方法。利用GC-MS联用、LC-MS联用分析技术对MDPV进行分析，得到MDPV的GC-MS分析主要特征离子及LC-MS联用分析分子离子峰、二级质谱碎片峰、三级质谱碎片峰，并对各特征离子及碎片峰进行了归属研究，得到了MDPV的GC-MS联用、LC-MS联用分析的质谱裂解规律及特征离子。
본문건립료책화약물아갑기이양필각무동（MDPV）적기상색보-질보（GC-MS）련용、액상색보-질보（LC-MS）련용분석방법。이용GC-MS련용、LC-MS련용분석기술대MDPV진행분석，득도MDPV적GC-MS분석주요특정리자급LC-MS련용분석분자리자봉、이급질보쇄편봉、삼급질보쇄편봉，병대각특정리자급쇄편봉진행료귀속연구，득도료MDPV적GC-MS련용、LC-MS련용분석적질보렬해규률급특정리자。
A method applying gas chromatography-mass spectrometry(GC-MS)and liquid chromatography-mass spec?trometry(LC-MS)for the analysis of designer drug methylenedioxy-pyrovalerone(MDPV)is described. MDPV was ana?lyzed by GC-MS and LC-MS. The character ions,parent ion and daughter ions of MDPV were all obtained and the rules of the analysis of MDPV by GC-MS and LC-MS were also discussed.