CAJ | 학술논문

建立了甜菜中5种有机氯农药残留的测定方法，样品以正己烷：丙酮（1：1）作为提取溶剂经快速溶剂萃取仪提取，再经Flo risil小柱（固相萃取柱）净化后，旋蒸至干，定容。对于甜菜这种复杂基质的样品，采用GC‐M S‐M S多反应监测（M RM ）方式进行定量和定性分析，可降低复杂基质的干扰，简化了分析步骤。加标水平分别为0.01、0.02、0.04 mg/kg时，回收率为89.5％～102.5％，符合农药残留检测的要求。用外标法定量，结果证明，该方法灵敏度高、快速、准确，适合甜菜中多种有机氯农药的检测。
건립료첨채중5충유궤록농약잔류적측정방법，양품이정기완：병동（1：1）작위제취용제경쾌속용제췌취의제취，재경Flo risil소주（고상췌취주）정화후，선증지간，정용。대우첨채저충복잡기질적양품，채용GC‐M S‐M S다반응감측（M RM ）방식진행정량화정성분석，가강저복잡기질적간우，간화료분석보취。가표수평분별위0.01、0.02、0.04 mg/kg시，회수솔위89.5％～102.5％，부합농약잔류검측적요구。용외표법정량，결과증명，해방법령민도고、쾌속、준학，괄합첨채중다충유궤록농약적검측。
An analytical method was established to determine five Organochlorine Pesticides residues in sugarbeet , the samples were extracted with n‐hexane‐acetone (1 :1 , V ;V) through accelerated Solvent extraction ,purified by Florisil solid phase extraction column ,concentrated by rotary evaporation ,brought to volume . Sugarbeet is a kind of complex matrix samples , so the detection of five Organochlorine Pesticides residues was carried out by GC‐MS‐MS in the multi‐reacting‐monitoring (MRM ) mode , minimized matrix interferences and simplied the analytical procedure . The recovery of the five Pesticides residues is about 89.5% ~102.5% when the add level is 0.01、0.02、0.04 mg/kg ,so the method accords with the demand for detection of Pesticides residues . The external reference method is used for quantify . The method is fast ,accurate and high sensitivity and it issuitable for determination of residual content of Organochlorine Pesticides in sugarbeet .