CAJ | 학술논문

通过正交表设计实验,利用高温高压釜腐蚀实验并辅以失重法,研究了温度、Cl-浓度、S2-浓度和HCO3-浓度对G105钻杆材料多元腐蚀行为的影响。采用体视显微镜和SEM观察腐蚀形态和产物膜形貌,同时利用X射线能谱分析仪（EDS）进行产物膜成分分析。结果表明,在实验研究范围内,NaHCO3浓度是最大的影响因素,其次是温度和Na2S浓度,NaCl浓度的影响最小;腐蚀环境严重影响腐蚀速率;在60℃,NaCl浓度为5g/L,Na2S浓度为7g/L以及NaHCO3浓度为1g/L环境下,G105钻杆材料的腐蚀以NaHCO3引起的腐蚀为主;在60℃,NaCl浓度为50g/L,Na2S浓度为30g/L以及NaHCO3浓度为30g/L环境下,G105钻杆材料的腐蚀以Na2S引起的腐蚀为主。
통과정교표설계실험,이용고온고압부부식실험병보이실중법,연구료온도、Cl-농도、S2-농도화HCO3-농도대G105찬간재료다원부식행위적영향。채용체시현미경화SEM관찰부식형태화산물막형모,동시이용X사선능보분석의（EDS）진행산물막성분분석。결과표명,재실험연구범위내,NaHCO3농도시최대적영향인소,기차시온도화Na2S농도,NaCl농도적영향최소;부식배경엄중영향부식속솔;재60℃,NaCl농도위5g/L,Na2S농도위7g/L이급NaHCO3농도위1g/L배경하,G105찬간재료적부식이NaHCO3인기적부식위주;재60℃,NaCl농도위50g/L,Na2S농도위30g/L이급NaHCO3농도위30g/L배경하,G105찬간재료적부식이Na2S인기적부식위주。
The influence of temperature, Cl- concentration, Se concentration and HCO3- concentration on G105 muhifaetor corrosion behavior was investigated by high temperature and pressure kettle with weight loss method in this paper. And the experiments were arranged with orthogonal table. The corrosion form and prod- uct topography were observed by stereomicroscope and SEM, and the composition of corrosion product was ana- lyzed by X-ray energy spectrum analyzer (EDS). The results show that, in the research range of this test, NaHCO3 concentration was the biggest factor, the second was temperature and Na2S concentration, while NaCl concentration was the minimum factor; corrosion environment seriously affects corrosion rate; at the tempera- ture of 60℃, when NaCl concentration was 5g/L, Na2S concentration was 7g/L and NaHCO3 concentration was 1g/L, the main corrosion of G105 drill pipe materials was caused by NaHCOa. At the temperature of 60℃, when NaCl concentration was 50g/L, Na2S concentration was 30g/L and NaHCO3 concentration was 30g/L, the corrosion was mainly caused by Na2S.