功能材料
功能材料
공능재료
JOURNAL OF FUNCTIONAL MATERIALS
2012年
24期
3456-3459
,共4页
李红云%修志亮%吴拥中%郝霄鹏
李紅雲%脩誌亮%吳擁中%郝霄鵬
리홍운%수지량%오옹중%학소붕
YVO4∶Eu空心球%自牺牲模板%光致发光
YVO4∶Eu空心毬%自犧牲模闆%光緻髮光
YVO4∶Eu공심구%자희생모판%광치발광
YVO4∶Eu hollow spheres%sacrificial template%photoluminescence
通过一步水热化学腐蚀YOHCO3∶Eu胶体微球制备了平均尺寸约为250nm的YVO4∶Eu空心球。利用XRD、SEM、EDS、TEM和PL等手段分别对YVO4∶Eu空心球的结构、形貌和发光性质进行了表征。在280nm紫外光激发下,YVO4∶Eu空心球在618nm处具有较强的红光发射。实验证明,YVO4∶Eu空心球的形成过程为溶液传质过程。
通過一步水熱化學腐蝕YOHCO3∶Eu膠體微毬製備瞭平均呎吋約為250nm的YVO4∶Eu空心毬。利用XRD、SEM、EDS、TEM和PL等手段分彆對YVO4∶Eu空心毬的結構、形貌和髮光性質進行瞭錶徵。在280nm紫外光激髮下,YVO4∶Eu空心毬在618nm處具有較彊的紅光髮射。實驗證明,YVO4∶Eu空心毬的形成過程為溶液傳質過程。
통과일보수열화학부식YOHCO3∶Eu효체미구제비료평균척촌약위250nm적YVO4∶Eu공심구。이용XRD、SEM、EDS、TEM화PL등수단분별대YVO4∶Eu공심구적결구、형모화발광성질진행료표정。재280nm자외광격발하,YVO4∶Eu공심구재618nm처구유교강적홍광발사。실험증명,YVO4∶Eu공심구적형성과정위용액전질과정。
Monodispersed YVO4∶Eu hollow microspheres with average diameters of 250 nm were successfully synthesized by one-pot hydrothermal treatment of YOHCO3∶Eu colloidal spheres.The structure,morphology,and photoluminescence properties were characterized by X-ray diffraction(XRD),scanning electron microscopy(SEM),energy-dispersive spectrometry(EDS),transmission electron microscopy(TEM),and photoluminescence(PL) spectrometer.The formation of the YVO4∶Eu hollow microspheres was revealed to be normal solution transport process.Under ultraviolet(280 nm) excitation,the YVO4∶Eu hollow microspheres showed strong red emission at 618 nm.