CAJ | 학술논문

以 D-氨基葡萄糖盐酸盐为起始原料，经过羟基的乙酰化保护，得到2-氨基-1，3，4，6-四-O-乙酰基-2-脱氧-β-D-吡喃糖盐酸盐；然后在三乙胺存在下，与三光气、哌嗪衍生物“一锅法”反应，合成4种具有代表性的糖基哌嗪物质。产物结构均经 FT-IR，1 H NMR 和 HRMS（ESI）确认。
이 D-안기포도당염산염위기시원료，경과간기적을선화보호，득도2-안기-1，3，4，6-사-O-을선기-2-탈양-β-D-필남당염산염；연후재삼을알존재하，여삼광기、고진연생물“일과법”반응，합성4충구유대표성적당기고진물질。산물결구균경 FT-IR，1 H NMR 화 HRMS（ESI）학인。
2-Amino-1,3,4,6-tetra-O-acetyl-2-deoxy-β-D-glucopyranose was synthesized by acetylation of hydroxy groups with D-glucosa as starting material.Under the catalysis of triethyla,four representative glycosylpiperazines were obtained via one-pot reaction of acetylglucosa,triphosgene and piperazine derivatives.The products were confirmed by FT-IR,1 H NMR and HRMS(ESI).