北方药学
北方藥學
북방약학
JOURNAL OF NORTH PHARMACY
2013年
4期
1-2
,共2页
减肥茶%ICP-MS%重金属%微波消解
減肥茶%ICP-MS%重金屬%微波消解
감비다%ICP-MS%중금속%미파소해
Weight-reducing tea%ICP-MS%Heavy metals%Microwave digestion
本文采用微波消解方法处理减肥茶样品后,用ICP-MS法测定样品中铅、汞、镉、砷、铜重金属元素的含量,通过优化ICP-MS仪器测定条件,用内标克服仪器信号漂移及样品基体效应等的影响,建立了ICP-MS法同时测定减肥茶中多种元素的方法,同时对市场上不同厂家及不同批次的7例样品重金属的污染状况进行了评估,为健康安全使用减肥茶提供有益参考.
本文採用微波消解方法處理減肥茶樣品後,用ICP-MS法測定樣品中鉛、汞、鎘、砷、銅重金屬元素的含量,通過優化ICP-MS儀器測定條件,用內標剋服儀器信號漂移及樣品基體效應等的影響,建立瞭ICP-MS法同時測定減肥茶中多種元素的方法,同時對市場上不同廠傢及不同批次的7例樣品重金屬的汙染狀況進行瞭評估,為健康安全使用減肥茶提供有益參攷.
본문채용미파소해방법처리감비다양품후,용ICP-MS법측정양품중연、홍、력、신、동중금속원소적함량,통과우화ICP-MS의기측정조건,용내표극복의기신호표이급양품기체효응등적영향,건립료ICP-MS법동시측정감비다중다충원소적방법,동시대시장상불동엄가급불동비차적7례양품중금속적오염상황진행료평고,위건강안전사용감비다제공유익삼고.
In this paper,microwave digestion approach to weight-reducing tea samples,with the weight-reducing tea by ICP-MS determination of lead,mercury,cadmium,arsenic,copper heavy metal content.By optimizing the conditions for ICP-MS instrument measured using an internal standard to overcome the instrument drift and sample matrix effects,the establishment of the ICP-MS method for simultaneous determination of many elements in weight-reducing tea.Furthermore, the contamination of heavy metals in severa1 commercial available weight-reducing teas were evaluated which can provide valuable references for the healthy.