中医药导报
中醫藥導報
중의약도보
GUIDING JOURNAL OF TCM
2013年
4期
68-69
,共2页
张京%李秀敏%孙世光%闫荟
張京%李秀敏%孫世光%閆薈
장경%리수민%손세광%염회
薄层%高效液相%紫外分光光度法
薄層%高效液相%紫外分光光度法
박층%고효액상%자외분광광도법
TLC%HPLC%UV spectrophotometry
目的:探讨复方选净散的质量标准.方法:采用TLC法对苦参进行定性鉴别;用紫外分光光度法对制剂中呋喃西林进行定量分析.结果:定量分析中呋喃西林检测浓度的线性范围为2.04-12.24μg/mL(r=0.9999,n=6);平均加样回收率为100.04%,RSD%=0.41%(n=6).结论:所建立的方法可靠、准确、专属性强,可控制该制剂的质量.
目的:探討複方選淨散的質量標準.方法:採用TLC法對苦參進行定性鑒彆;用紫外分光光度法對製劑中呋喃西林進行定量分析.結果:定量分析中呋喃西林檢測濃度的線性範圍為2.04-12.24μg/mL(r=0.9999,n=6);平均加樣迴收率為100.04%,RSD%=0.41%(n=6).結論:所建立的方法可靠、準確、專屬性彊,可控製該製劑的質量.
목적:탐토복방선정산적질량표준.방법:채용TLC법대고삼진행정성감별;용자외분광광도법대제제중부남서림진행정량분석.결과:정량분석중부남서림검측농도적선성범위위2.04-12.24μg/mL(r=0.9999,n=6);평균가양회수솔위100.04%,RSD%=0.41%(n=6).결론:소건립적방법가고、준학、전속성강,가공제해제제적질량.
@@@@ Objective: To explore the Quality Standard for Fu-fang Xuan-jing powder. Methods: TLC method was applied for qualitative identification of Sophora flavescens; ultraviolet spectrophotometric method was used for preparation of nitrofura-zone quantitative analysis. Results: In the quantitative analysis of nitrofurazone detection concentration, the linear range of 2.04-12.24 μg/mL(r=0.9999, n=6), and the average recovery was 100.04%; RSD%=0.41%(n=6). Conclusion: This method is re-liable, accurate and specific for the quality control of the preparation.