北京科技大学学报
北京科技大學學報
북경과기대학학보
JOURNAL OF UNIVERSITY OF SCIENCE AND TECHNOLOGY BEIJING
2013年
3期
304-311
,共8页
齐亮%赵征志%赵爱民%黄耀
齊亮%趙徵誌%趙愛民%黃耀
제량%조정지%조애민%황요
管线钢%析出%晶粒长大%奥氏体%碳氮化物%动力学
管線鋼%析齣%晶粒長大%奧氏體%碳氮化物%動力學
관선강%석출%정립장대%오씨체%탄담화물%동역학
pipeline steel%precipitation%grain growth%austenite%carbonitrides%kinetics
基于双亚点阵模型,计算了两种不同铌含量的高钢级管线钢在不同温度下 Nb、Ti 和 Al 的析出量,测定了不同加热温度和保温时间下奥氏体晶粒尺寸,建立两种钢奥氏体晶粒长大模型.发现 Nb 含量增加提高了其全固溶温度,并且温降过程中 Nb 析出量显著增多,在晶界两边析出的细小碳氮化物对奥氏体晶粒长大有显著的阻碍作用.高铌钢加热温度为1250℃时奥氏体晶粒显著粗化,预测模型也不同于1050~1200℃的模型,但相同保温温度下晶粒尺寸明显小于低铌实验钢.通过数据拟合计算出高铌钢的长大激活能远远高于低铌钢,再次证明高 Nb 的管线钢在1200℃以下能够有效地细化奥氏体晶粒,预测模型与实验值吻合较好.
基于雙亞點陣模型,計算瞭兩種不同鈮含量的高鋼級管線鋼在不同溫度下 Nb、Ti 和 Al 的析齣量,測定瞭不同加熱溫度和保溫時間下奧氏體晶粒呎吋,建立兩種鋼奧氏體晶粒長大模型.髮現 Nb 含量增加提高瞭其全固溶溫度,併且溫降過程中 Nb 析齣量顯著增多,在晶界兩邊析齣的細小碳氮化物對奧氏體晶粒長大有顯著的阻礙作用.高鈮鋼加熱溫度為1250℃時奧氏體晶粒顯著粗化,預測模型也不同于1050~1200℃的模型,但相同保溫溫度下晶粒呎吋明顯小于低鈮實驗鋼.通過數據擬閤計算齣高鈮鋼的長大激活能遠遠高于低鈮鋼,再次證明高 Nb 的管線鋼在1200℃以下能夠有效地細化奧氏體晶粒,預測模型與實驗值吻閤較好.
기우쌍아점진모형,계산료량충불동니함량적고강급관선강재불동온도하 Nb、Ti 화 Al 적석출량,측정료불동가열온도화보온시간하오씨체정립척촌,건립량충강오씨체정립장대모형.발현 Nb 함량증가제고료기전고용온도,병차온강과정중 Nb 석출량현저증다,재정계량변석출적세소탄담화물대오씨체정립장대유현저적조애작용.고니강가열온도위1250℃시오씨체정립현저조화,예측모형야불동우1050~1200℃적모형,단상동보온온도하정립척촌명현소우저니실험강.통과수거의합계산출고니강적장대격활능원원고우저니강,재차증명고 Nb 적관선강재1200℃이하능구유효지세화오씨체정립,예측모형여실험치문합교호.
@@@@Based on the double-sublattice model, the mass fractions of Nb, Ti and Al precipitates in two high-grade pipeline steels were calculated at different temperatures. The sizes of austenite grains in the two steels were determined at different heating temperatures after different soaking time. Two models were built to describe the austenite grain growth. It is found that the complete-solution temperature increases with the addition of Nb. The amount of small carbonitrides at the sides of grain boundaries, which hinder the austenite grain growth, also increases due to the drop of temperature. Austenite grains in the high-Nb steel remarkably coarsen when the soaking temperature is 1250 ℃, the prediction model is different from those used between 1050 and 1200 ℃, but the austenite grain size is obviously smaller than that of the low-Nb steel at the same soaking temperature. Based on the data-fit method, the austenite-growth activation energy of the high-Nb steel is calculated, which is much larger than that of the low-Nb steel. It is again proved that austenite grains are greatly refined in the high-Nb pipeline steel soaked at temperatures no more than 1200 ℃. The prediction models show good agreement with experimental data.