食品与药品
食品與藥品
식품여약품
FOOD AND DRUG
2012年
5期
162-164
,共3页
孙敬勇%孙洁%武海艳%刘珂
孫敬勇%孫潔%武海豔%劉珂
손경용%손길%무해염%류가
山香圆叶%化学成分%结构鉴定
山香圓葉%化學成分%結構鑒定
산향원협%화학성분%결구감정
Turpiniae Folium%chemical constituents%structure identification
目的研究山香圆叶的化学成分.方法采用色谱技术进行分离、纯化,通过理化常数和波谱分析鉴定化合物结构.结果从山香圆叶中分离出10个化合物,分别为芹菜素(1),芹菜素-7-O-β-D-葡糖苷(2),芹菜素-7-新橙皮糖苷(3),芹菜素-7-(2′-α-L-鼠李糖基)芸香糖苷(4),对羟基桂皮酸(5),没食子酸乙酯(6),没食子酸(7),eucomic acid(8),β-谷甾醇(9),胡萝卜苷(10).结论化合物4~6,8,9为首次从该属植物中分离得到.
目的研究山香圓葉的化學成分.方法採用色譜技術進行分離、純化,通過理化常數和波譜分析鑒定化閤物結構.結果從山香圓葉中分離齣10箇化閤物,分彆為芹菜素(1),芹菜素-7-O-β-D-葡糖苷(2),芹菜素-7-新橙皮糖苷(3),芹菜素-7-(2′-α-L-鼠李糖基)蕓香糖苷(4),對羥基桂皮痠(5),沒食子痠乙酯(6),沒食子痠(7),eucomic acid(8),β-穀甾醇(9),鬍蘿蔔苷(10).結論化閤物4~6,8,9為首次從該屬植物中分離得到.
목적연구산향원협적화학성분.방법채용색보기술진행분리、순화,통과이화상수화파보분석감정화합물결구.결과종산향원협중분리출10개화합물,분별위근채소(1),근채소-7-O-β-D-포당감(2),근채소-7-신등피당감(3),근채소-7-(2′-α-L-서리당기)예향당감(4),대간기계피산(5),몰식자산을지(6),몰식자산(7),eucomic acid(8),β-곡치순(9),호라복감(10).결론화합물4~6,8,9위수차종해속식물중분리득도.
@@@@Objective To study the chemical constituents of Turpiniae Folium. Methods The compounds were isolated and purified by column chromatography and their structures were identified on the basis of physicochemical properties and spectral analyses. Results Ten compounds were isolated and their structures were identified as apigenin( 1), apigenin 7-O-β-D-glucoside( 2), apigenin 7-neohesperidoside( 3), apigenin 7-(2′-rhamnosyl) rotinoside( 4), p-hydroxycinnamic acid( 5), galic acid ethyl ester( 6), galic acid( 7), eucomic acid( 8), β-sitosterol( 9), daucostero( 10). Conclusion The compounds 4~6, 8, 9 were isolated and identified from this genus for the first time.