中医药导报
中醫藥導報
중의약도보
GUIDING JOURNAL OF TCM
2013年
2期
97-98
,共2页
吴樱%贾安%周海凤%倪卫民
吳櫻%賈安%週海鳳%倪衛民
오앵%가안%주해봉%예위민
三黄止痒搽剂%高效薄层色谱法%定性鉴别
三黃止癢搽劑%高效薄層色譜法%定性鑒彆
삼황지양차제%고효박층색보법%정성감별
Sanhuang Liniment%HPTLC%Qualitative identification
目的:建立三黄止痒搽剂的薄层定性鉴别方法.方法:采用HPTLC法,以不同展开系统分别对处方中黄柏、黄芩、大黄、苦参进行薄层定性鉴别.结果:HPTLC的斑点清晰、分离度较好.处方样品中斑点与对照品中斑点Rf值一致,阴性无干扰.结论:所建立的方法对方中的药材可准确、快速地进行定性检测,可用于三黄止痒捈剂的质量控制.
目的:建立三黃止癢搽劑的薄層定性鑒彆方法.方法:採用HPTLC法,以不同展開繫統分彆對處方中黃柏、黃芩、大黃、苦參進行薄層定性鑒彆.結果:HPTLC的斑點清晰、分離度較好.處方樣品中斑點與對照品中斑點Rf值一緻,陰性無榦擾.結論:所建立的方法對方中的藥材可準確、快速地進行定性檢測,可用于三黃止癢捈劑的質量控製.
목적:건립삼황지양차제적박층정성감별방법.방법:채용HPTLC법,이불동전개계통분별대처방중황백、황금、대황、고삼진행박층정성감별.결과:HPTLC적반점청석、분리도교호.처방양품중반점여대조품중반점Rf치일치,음성무간우.결론:소건립적방법대방중적약재가준학、쾌속지진행정성검측,가용우삼황지양도제적질량공제.
Objective: To establish a method of high performance thin layer chromatography (HPTLC) for identifying the qualitation of Sanhuang liniment. Methods: Identified the Amur Corktree Bark, Baikal Skullcap Root, Rhubarb and Lightyellow Sophora Root in the prescription of Sanhuang Liniment by different development system with HPTLC. Results: The spots appeared clear and the resolution was satisfactory. The Rf values of spots of prescription samples were consistent with those of reference substance. There is no negative interference. Conclusion: The method is proved to be sensitive and precise, and can be used for the quality control of Sanhuang liniment.