化学通报（网络版）
化學通報（網絡版）
화학통보（망락판）
Chemistry Online
2003年
1期
,共1页
减压柱层析%分离纯化%新杀虫剂HNPC-A9835%新药创制
減壓柱層析%分離純化%新殺蟲劑HNPC-A9835%新藥創製
감압주층석%분리순화%신살충제HNPC-A9835%신약창제
Pressure reducing column chromatography(PRCC)%Separation and purification%New pesticide HNPC-A9835%Formulation of new pesticides
研究了减压柱层析分离纯化方法在新药合成中的应用.利用薄层层析硅胶H为吸附剂,石油醚和乙酸乙酯为混合洗脱剂,通过减压柱层析,分离纯化新型杀虫剂HNPC-A9835,纯度达96.72%.减压柱层析分离纯化方法具有快速、简便的特点,并可达到理想的分离效果.
研究瞭減壓柱層析分離純化方法在新藥閤成中的應用.利用薄層層析硅膠H為吸附劑,石油醚和乙痠乙酯為混閤洗脫劑,通過減壓柱層析,分離純化新型殺蟲劑HNPC-A9835,純度達96.72%.減壓柱層析分離純化方法具有快速、簡便的特點,併可達到理想的分離效果.
연구료감압주층석분리순화방법재신약합성중적응용.이용박층층석규효H위흡부제,석유미화을산을지위혼합세탈제,통과감압주층석,분리순화신형살충제HNPC-A9835,순도체96.72%.감압주층석분리순화방법구유쾌속、간편적특점,병가체도이상적분리효과.
The application of pressure reducing column chromatography(PRCC) in the formulation of new pesticides has been studied. Using silica gel H for thin-layer chromatography(TLC) as absorbent and petroleum ether and ethyl acetate as mixed washing agent, New pesticide HNPC-A9835 has been separated and purified with the content of 96.72% by PRCC, the method of PRCC is rapid and simple and its result is desirable.
