食品与药品
食品與藥品
식품여약품
FOOD AND DRUG
2012年
11期
422-423
,共2页
宋军%王鹏程%李艳%姜立会
宋軍%王鵬程%李豔%薑立會
송군%왕붕정%리염%강립회
黑升麻苷%提取工艺%正交试验
黑升痳苷%提取工藝%正交試驗
흑승마감%제취공예%정교시험
black cohosh glycosides%extraction%orthogonal test
目的确定黑升麻苷的最佳提取工艺.方法正交试验设计优选条件,HPLC法测定黑升麻提取液中黑升麻苷含量.结果优选工艺为黑升麻药材加10倍量60%乙醇回流提取,提取3次,每次1.5 h.结论优化选择的提取工艺较稳定,重现性好,可为生产实践提供理论依据.
目的確定黑升痳苷的最佳提取工藝.方法正交試驗設計優選條件,HPLC法測定黑升痳提取液中黑升痳苷含量.結果優選工藝為黑升痳藥材加10倍量60%乙醇迴流提取,提取3次,每次1.5 h.結論優化選擇的提取工藝較穩定,重現性好,可為生產實踐提供理論依據.
목적학정흑승마감적최가제취공예.방법정교시험설계우선조건,HPLC법측정흑승마제취액중흑승마감함량.결과우선공예위흑승마약재가10배량60%을순회류제취,제취3차,매차1.5 h.결론우화선택적제취공예교은정,중현성호,가위생산실천제공이론의거.
Objective To optimize the extraction process of black cohosh. Methods Orthogonal tests were design for optimum conditions, with HPLC method for the determination of black cohosh glycoside in black cohosh extract. Results Optimum process was black cohosh herbal add 10 volume of 60 % ethanol, refluxing extraction for 3 times, each 1.5 h. Conclusion Optimized process is stable and reproducible, providing theoretical basis for production practice.
