CAJ | 학술논문

采用水蒸气蒸馏法提取闽楠果皮挥发油,并用气相色谱-质谱联用技术对其果皮挥发油的化学成分进行分离鉴定,利用峰面积归一化法确定各组分的相对含量.从检出的87种成分中鉴定出55种,所鉴定成分占总挥发油量的74.42%,其主要化学成分为α-水芹烯(9.18%)、杜松烯(6.41%)、α-石竹烯(6.23%)、(-)-4-萜品醇(4.47%)、大根香叶烯(3.45%)、异龙脑(3.34%)、(-)-桉叶烯醇(3.28%)、(-)-α-桉烯(3.24%)、1-石竹烯(3.10%)、樟脑(2.76%)、(-)-可巴烯(2.63%)、乙酸龙脑酯(2.61%)、2-β-薄荷二烯(1.90%)、β-榄香烯(1.32%)、绿花白千层醇(1.25%)、1(5)-愈创木烯-11-醇(1.27%)等.
채용수증기증류법제취민남과피휘발유,병용기상색보-질보련용기술대기과피휘발유적화학성분진행분리감정,이용봉면적귀일화법학정각조분적상대함량.종검출적87충성분중감정출55충,소감정성분점총휘발유량적74.42%,기주요화학성분위α-수근희(9.18%)、두송희(6.41%)、α-석죽희(6.23%)、(-)-4-첩품순(4.47%)、대근향협희(3.45%)、이용뇌(3.34%)、(-)-안협희순(3.28%)、(-)-α-안희(3.24%)、1-석죽희(3.10%)、장뇌(2.76%)、(-)-가파희(2.63%)、을산용뇌지(2.61%)、2-β-박하이희(1.90%)、β-람향희(1.32%)、록화백천층순(1.25%)、1(5)-유창목희-11-순(1.27%)등.
The volatile oil from the peel of Phoebe bournei was extracted by steam distillation method, its chemical constituents were identified by means of GC-MS, and the relative amounts of those constituents were determined by peak area normalization method. The result showed that 55 among 87 constituents were identified and quantified for 74.42%of the total volatile oil. The main constituents areα-Phellandrene (9.18%), Cadinene (6.41%), α-Carophyllene (6.23%), (-)-4-Terpineol (4.47%), Germacrene (3.45%), Isoborneol (3.34%), (-)-Spathulenol (3.28%), (-)-α-Selinene (3.24%), l-Caryophyllene (3.10%), Camphor (2.76%), (-)-Copaene (2.63%), Bornyl acetate (2.61%), 2-β-menthadiene (1.90%), β-Elemene (1.32%), Viridiflorol (1.25%), 1(5)-guaienyl-11-ol (1.27%).