CAJ | 학술논문

通过光学显微观察(OM)、扫描电镜观察(SEM)、透射电镜观察(TEM)、X 射线衍射(XRD)及力学性能测试等方法,研究 Mg-0.5%Zn-0.5%Ce-0.5%Zr 合金在温度为400℃,轧制速率为10 m/min,道次压下量分别为20%、30%和50%条件下轧制及退火后的微观组织及力学性能.结果表明:在400℃,以不同道次压下量轧制后,合金发生了不同程度的动态回复,且道次压下量为50%时,轧制后的合金中包含了更多的位错结构.轧制后合金主要呈现典型的{0001}基面织构,且采用大道次压下量轧制的合金的基面织构较强.轧制合金经500℃退火后,发生了明显的静态再结晶,退火后组织的{0001}基面织构明显减弱,这主要由于静态再结晶后晶粒取向发生转变,弱化了基面织构.由于织构的存在,轧制态合金表现出明显的各向异性;退火后,由于织构弱化,合金的各向异性得到明显改善.
통과광학현미관찰(OM)、소묘전경관찰(SEM)、투사전경관찰(TEM)、X 사선연사(XRD)급역학성능측시등방법,연구 Mg-0.5%Zn-0.5%Ce-0.5%Zr 합금재온도위400℃,알제속솔위10 m/min,도차압하량분별위20%、30%화50%조건하알제급퇴화후적미관조직급역학성능.결과표명:재400℃,이불동도차압하량알제후,합금발생료불동정도적동태회복,차도차압하량위50%시,알제후적합금중포함료경다적위착결구.알제후합금주요정현전형적{0001}기면직구,차채용대도차압하량알제적합금적기면직구교강.알제합금경500℃퇴화후,발생료명현적정태재결정,퇴화후조직적{0001}기면직구명현감약,저주요유우정태재결정후정립취향발생전변,약화료기면직구.유우직구적존재,알제태합금표현출명현적각향이성;퇴화후,유우직구약화,합금적각향이성득도명현개선.
The microstructures and mechanical properties of rolled Mg-0.5%Zn-0.5%Ce-0.5%Zr alloy were investigated. The alloy was rolled with different per-pass reductions (20%, 30%, 50%) at 400 ℃ and run speed of 10 m/min. The microstructures were observed by OM, SEM, TEM and XRD. The results show that only dynamic recovery (DRV) takes place in Mg-Zn-Ce-Zr alloy during rolling at 400 ℃ with various per-pass reductions. Meanwhile, more dislocations are found in 50% per-pass reduction rolled alloy. The overall texture intensity of {0001} basal plane is weaker for 20%per-pass reduction rolled alloys compared to 30% or 50%. After annealing at 500 ℃, the static recrystallization occurs in Mg-Zn-Ce-Zr alloy sheets. Texture weakening also happens after annealing, this is attributed to grain rotation during static recrystallization. Obvious anisotropy is found in the rolled alloys due to the basal texture, and then the anisotropy is weakened by texture randomization.