中国医药导刊
中國醫藥導刊
중국의약도간
CHINESE JOURNAL OF MEDICAL GUIDE
2012年
z2期
785-787
,共3页
奚建%李建利*%施明毅%谢燕%杨珊%王利洁
奚建%李建利*%施明毅%謝燕%楊珊%王利潔
해건%리건리*%시명의%사연%양산%왕리길
正交设计%蛇床子素含量%高效液相色谱法
正交設計%蛇床子素含量%高效液相色譜法
정교설계%사상자소함량%고효액상색보법
orthogonal design%Osthol%high performance liquid chromatography
目的:优选痹痛贴最佳提取工艺.方法:以乙醇浓度、乙醇用量、提取时间、提取次数为考察因素,用L9(34)正交试验表安排正交试验,以蛇床子素含量、干膏收率为考察指标,采用综合加权评分法进行数据分析,优化独活、川芎、川木香、乳香、没药等药的乙醇回流提取工艺条件.结果:最佳工艺为药材加70%乙醇回流提取2次,每次1h,第一次加醇量为8倍,第二次加醇量为6倍.结论:该工艺客观可行,稳定合理,可为工业化生产提供理论依据.
目的:優選痺痛貼最佳提取工藝.方法:以乙醇濃度、乙醇用量、提取時間、提取次數為攷察因素,用L9(34)正交試驗錶安排正交試驗,以蛇床子素含量、榦膏收率為攷察指標,採用綜閤加權評分法進行數據分析,優化獨活、川芎、川木香、乳香、沒藥等藥的乙醇迴流提取工藝條件.結果:最佳工藝為藥材加70%乙醇迴流提取2次,每次1h,第一次加醇量為8倍,第二次加醇量為6倍.結論:該工藝客觀可行,穩定閤理,可為工業化生產提供理論依據.
목적:우선비통첩최가제취공예.방법:이을순농도、을순용량、제취시간、제취차수위고찰인소,용L9(34)정교시험표안배정교시험,이사상자소함량、간고수솔위고찰지표,채용종합가권평분법진행수거분석,우화독활、천궁、천목향、유향、몰약등약적을순회류제취공예조건.결과:최가공예위약재가70%을순회류제취2차,매차1h,제일차가순량위8배,제이차가순량위6배.결론:해공예객관가행,은정합리,가위공업화생산제공이론의거.
Objective: to optimize the best extraction process of arthralgia paste. Methods: ethanol concentration, ethanol concentration, extraction time, extraction times as factors, L9 ( 34 ) orthogonal test table of orthogonal test, the target of Osthol content, yield of dry extract, using the synthetic weighted mark method for data analysis, extraction condition optimization of angelica, chuanxiong, ethanol reflux Kawa Kika, frankincense, myrrh medicine. Results: the best process were as follows: 70%ethanol reflux extraction 2 times, each time 1H, the first time the amount of alcohol for 8 times, second times the amount of alcohol for 6 times. Conclusion: the process is feasible, stable and reasonable, which can provide the theoretical basis for the industrial production of.