医药前沿
醫藥前沿
의약전연
YIAYAO QIANYAN
2013年
12期
53-55
,共3页
劳燕霞%宋丽莉%陈燕霞%徐小飞%陈康%黎珊%苏昭仑
勞燕霞%宋麗莉%陳燕霞%徐小飛%陳康%黎珊%囌昭崙
로연하%송려리%진연하%서소비%진강%려산%소소륜
款冬花%炮制%挥发油%GC-MS
款鼕花%砲製%揮髮油%GC-MS
관동화%포제%휘발유%GC-MS
Flos Farfarae%Volatile%Oil Processing%GC-MS
目的对款冬花蜜炙前后挥发油中化学成分的变化进行定性定量分析,为探讨其炮制原理提供实验基础.方法采用传统的水蒸气蒸馏法提取款冬花及其蜜炙品中的挥发油,并应用气质联用(GC-MS)技术分析所提取的挥发油化学成分.结果蜜炙前后共有的化合物20种,蜜炙后有11种化合物未被检出,新检出6种化合物;9种化合物蜜炙后相对含量增加,11种化合物相对含量减少.结论蜜炙不仅可使款冬花的挥发油发生量的变化,也能使其发生质的变化,这为款冬花炮制后药性改变和不同的临床应用研究提供了一定的理论依据.
目的對款鼕花蜜炙前後揮髮油中化學成分的變化進行定性定量分析,為探討其砲製原理提供實驗基礎.方法採用傳統的水蒸氣蒸餾法提取款鼕花及其蜜炙品中的揮髮油,併應用氣質聯用(GC-MS)技術分析所提取的揮髮油化學成分.結果蜜炙前後共有的化閤物20種,蜜炙後有11種化閤物未被檢齣,新檢齣6種化閤物;9種化閤物蜜炙後相對含量增加,11種化閤物相對含量減少.結論蜜炙不僅可使款鼕花的揮髮油髮生量的變化,也能使其髮生質的變化,這為款鼕花砲製後藥性改變和不同的臨床應用研究提供瞭一定的理論依據.
목적대관동화밀자전후휘발유중화학성분적변화진행정성정량분석,위탐토기포제원리제공실험기출.방법채용전통적수증기증류법제취관동화급기밀자품중적휘발유,병응용기질련용(GC-MS)기술분석소제취적휘발유화학성분.결과밀자전후공유적화합물20충,밀자후유11충화합물미피검출,신검출6충화합물;9충화합물밀자후상대함량증가,11충화합물상대함량감소.결론밀자불부가사관동화적휘발유발생량적변화,야능사기발생질적변화,저위관동화포제후약성개변화불동적림상응용연구제공료일정적이론의거.
Objective Analysis the change of components in the volatile oil of Flos Farfarae before and after stir-fried with honey to provide experimental data for discussing the principle of stir-fried with honey . Methods Extracted the volatile oil of Flos Farfarae before and after stir-fried with honey by Steam distilation , then analysis the extractions by GC-MS. Results 20 kinds of components in volatile Oil of Flos Farfarae before and after after stir-fried with honey were the same,11species were not detected after stir-fried with honey , but there are 6 kinds of new detection. 9 kinds of the relative contents increased ,11 kinds decreased. Conclusion There is a big difference between the components in the volatile oil after stir-fried with honey, and the content of the components also have changed . This artical may offer some theoretical evidences for drug property transform and different clinical application on Flos Farfarae after stir-fried with honey .