CAJ | 학술논문

建立了制备氮气中六氟化硫气体标准物质的方法。以称量法制备气体标准物质并计算定值，采用气相色谱法对制备的气体标准物质的均匀性和稳定性进行考察。将所制备的标准物质与中国计量院提供的氮气中六氟化硫气体标准物质进行比对分析验证，确保了气体标准物质量值的准确可靠。结果表明，所研制的浓度为10μL／L 的氮气中六氟化硫气体标准物质定值的扩展不确定度为2%，贮存有效期为1 年，完全能够满足电力部门仪表的检定与校准要求。
건립료제비담기중륙불화류기체표준물질적방법。이칭량법제비기체표준물질병계산정치，채용기상색보법대제비적기체표준물질적균균성화은정성진행고찰。장소제비적표준물질여중국계량원제공적담기중륙불화류기체표준물질진행비대분석험증，학보료기체표준물질량치적준학가고。결과표명，소연제적농도위10μL／L 적담기중륙불화류기체표준물질정치적확전불학정도위2%，저존유효기위1 년，완전능구만족전력부문의표적검정여교준요구。
The method for preparing sulfur hexafluoride in nitrogen gas reference material was set up. Gas reference material was prepared by weighting method and the value of the gas constant was calculated,uniformity and stability of gas reference material prepared were investigated by using gas chromatography. Sulfur hexafluoride in nitrogen gas reference material was compared with that provided by China Institute of Metrology to verify and ensure the accuracy of the reliability of gas reference material. The results showed that the developed concentration 10 μL/L expanded uncertainty of the sulfur hexafluoride in nitrogen gas reference material given value was 2%,storage valid for one year,fully able to meet the electricity sector instruments test and calibration requirement.