中国药业
中國藥業
중국약업
CHINA PHARMACEUTICALS
2014年
22期
45-46,47
,共3页
董超琪%袁华峰%屈蓉
董超琪%袁華峰%屈蓉
동초기%원화봉%굴용
高效液相色谱法%注射用头孢曲松钠%不确定度
高效液相色譜法%註射用頭孢麯鬆鈉%不確定度
고효액상색보법%주사용두포곡송납%불학정도
HPLC%Ceftriaxone Sodium for Injection%uncertainty
目的：对高效液相色谱法测定注射用头孢曲松钠含量的测量不确定度进行评定，以期找出影响不确定度的因素。方法按照测量步骤，并根据《测量不确定度评定与表示）（JJF1059－1999）中有关规定评估其不确定度。结果量化各不确定度分量，提出了该法的合成不确定度评估结果。结论计算出的扩展不确定度 U=1.3%，k=2。
目的：對高效液相色譜法測定註射用頭孢麯鬆鈉含量的測量不確定度進行評定，以期找齣影響不確定度的因素。方法按照測量步驟，併根據《測量不確定度評定與錶示）（JJF1059－1999）中有關規定評估其不確定度。結果量化各不確定度分量，提齣瞭該法的閤成不確定度評估結果。結論計算齣的擴展不確定度 U=1.3%，k=2。
목적：대고효액상색보법측정주사용두포곡송납함량적측량불학정도진행평정，이기조출영향불학정도적인소。방법안조측량보취，병근거《측량불학정도평정여표시）（JJF1059－1999）중유관규정평고기불학정도。결과양화각불학정도분량，제출료해법적합성불학정도평고결과。결론계산출적확전불학정도 U=1.3%，k=2。
Objective To evaluate and analyze the uncertainty of Ceftriaxone Sodium for Injection determined by high performance liquid chromatography ( HPLC ) in order to find out the factors influencing the uncertainty. Methods According to the measurement procedure and the Evaluation and Expression of Uncertainty in Measurement(JJF1059-1999),the measurement uncertainty was evaluated. Results The various components of uncertainties were quantified and the evaluation result of the synthesized uncertainty for this method was proposed. Conclusion The expanded uncertainty U=1. 3%( k=2)is calculated.
