CAJ | 학술논문

采用带捕集肼的静态顶空与固相微萃取法分别测定元宝枫叶片挥发物成分，通过气相色谱-质谱联用仪定性和定量分析，对两种方法进行比较。结果表明，静态顶空检测的成分较少，固相微萃取法检测的成分较多，但均以酯类和萜烯类物质为主。两种方法共同检测出的成分有10种，分别为3-己烯醇、乙酸叶醇酯、乙酸己酯、2-己烯-1-醇乙酸酯、柠檬腈、丁酸-4-己烯酯、丁酸-3-己烯酯、丁酸己酯、β-石竹烯和α-石竹烯。两种方法检测到的挥发物的相对含量差异较大。通过比较来看，采用SPME法更适合元宝枫叶片挥发物的测定。
채용대포집정적정태정공여고상미췌취법분별측정원보풍협편휘발물성분，통과기상색보-질보련용의정성화정량분석，대량충방법진행비교。결과표명，정태정공검측적성분교소，고상미췌취법검측적성분교다，단균이지류화첩희류물질위주。량충방법공동검측출적성분유10충，분별위3-기희순、을산협순지、을산기지、2-기희-1-순을산지、저몽정、정산-4-기희지、정산-3-기희지、정산기지、β-석죽희화α-석죽희。량충방법검측도적휘발물적상대함량차이교대。통과비교래간，채용SPME법경괄합원보풍협편휘발물적측정。
Volatiles from leaves of Acer truncatum Bunge were extracted by Static Headspace (SHS) and Solid-phase Microextraction (SPME) respectively. Their qualitative and quantitative analysis of volatiles was carried out by GC/MS. The results indicated that more compounds were identified by SPME, while that of SHS was fewer. 3-Hexen-1-ol, 3-Hexen-1-ol,acetate, Acetic acid hexyl ester, 2-Hexen-1-ol,acetate, Geranyl nitrile, Butanoic acid, 4-Hexenyl ester, Butanoic acid, 3-Hexenyl ester, Butanoic acid hexyl ester, β-Caryophyllene andα-Caryophyllene were identified by SHS and SPME simultaneously. The results showed that SPME was more suitable for the analysis of Volatiles from Leaves of Acer truncatum Bunge.