黑龙江医药
黑龍江醫藥
흑룡강의약
HEILONGJIANG MEDICAL JOURNAL
2014年
6期
1277-1277,1278
,共2页
保元胶囊Ⅰ%丹酚酸B%高效液相
保元膠囊Ⅰ%丹酚痠B%高效液相
보원효낭Ⅰ%단분산B%고효액상
Baoyuan capsuleⅠ%Salvianolic acid B%HPLC
目的：建立高效液相法测定保元胶囊Ⅰ中丹酚酸B的含量。方法：色谱柱为Angilent C18柱；流动相：甲醇-乙腈-甲酸-水(30：10：1：59)，检测波长为286nm；流速为1.0ml/min。结果：丹酚酸B线性范围10.28～61.68μg·mL-1，平均回收率为100.0%，RSD=0.5%。结论：方法简便，结果准确。能有效控制保元胶囊Ⅰ的质量。
目的：建立高效液相法測定保元膠囊Ⅰ中丹酚痠B的含量。方法：色譜柱為Angilent C18柱；流動相：甲醇-乙腈-甲痠-水(30：10：1：59)，檢測波長為286nm；流速為1.0ml/min。結果：丹酚痠B線性範圍10.28～61.68μg·mL-1，平均迴收率為100.0%，RSD=0.5%。結論：方法簡便，結果準確。能有效控製保元膠囊Ⅰ的質量。
목적：건립고효액상법측정보원효낭Ⅰ중단분산B적함량。방법：색보주위Angilent C18주；류동상：갑순-을정-갑산-수(30：10：1：59)，검측파장위286nm；류속위1.0ml/min。결과：단분산B선성범위10.28～61.68μg·mL-1，평균회수솔위100.0%，RSD=0.5%。결론：방법간편，결과준학。능유효공제보원효낭Ⅰ적질량。
Objective:To determine the content of Salvianolic acid B by HPLC in Baoyuan CapsuleⅠ. Methods:The determina-tion was carried out with Angilent C18 column.The mobile phase.consisted of CH3OH-CH3CN-HCOOH-H2O (30:10:1:59) . The flow rate was 1ml/min and the detective wavelength was at 286nm. Results:The content of Salvianolic acid B can be determined by HPLC. The linear concentration range of Salvianolic acid B was 10.28~61.68μg/ml. The average recovery was 100.0%respectively. Conclu-tion:The method is simple and accurate and can be used to control quality of Baoyuan capsuleⅠ.
