功能材料
功能材料
공능재료
JOURNAL OF FUNCTIONAL MATERIALS
2014年
24期
24131-24135,24139
,共6页
张力%赵玉涛%贾志宏%梁向锋
張力%趙玉濤%賈誌宏%樑嚮鋒
장력%조옥도%가지굉%량향봉
单晶高温合金%再结晶%压痕%热裂
單晶高溫閤金%再結晶%壓痕%熱裂
단정고온합금%재결정%압흔%열렬
single crystal superalloy%recrystallization%indentation%heat cracking
在不同热处理温度和载荷下,研究了 CM-SX-6单晶的再结晶现象。结果表明:在低于1150℃×4 h热处理后,没发现再结晶现象,但在载荷的作用下,单晶退火时γ'相形成元素自发偏析,造成大量的大颗粒γ'相在共晶周围析出;随着热处理温度升高,载荷影响区再结晶经历由压痕周围胞状再结晶、枝晶干再结晶、多个等轴再结晶三个阶段;在高于1150℃×4 h热处理时,单晶随着载荷的增加,再结晶的范围和深度明显增大;以及随冷却速率的增加,再结晶晶粒之间的热裂倾向增大,致使大量热裂沿晶界分布。
在不同熱處理溫度和載荷下,研究瞭 CM-SX-6單晶的再結晶現象。結果錶明:在低于1150℃×4 h熱處理後,沒髮現再結晶現象,但在載荷的作用下,單晶退火時γ'相形成元素自髮偏析,造成大量的大顆粒γ'相在共晶週圍析齣;隨著熱處理溫度升高,載荷影響區再結晶經歷由壓痕週圍胞狀再結晶、枝晶榦再結晶、多箇等軸再結晶三箇階段;在高于1150℃×4 h熱處理時,單晶隨著載荷的增加,再結晶的範圍和深度明顯增大;以及隨冷卻速率的增加,再結晶晶粒之間的熱裂傾嚮增大,緻使大量熱裂沿晶界分佈。
재불동열처리온도화재하하,연구료 CM-SX-6단정적재결정현상。결과표명:재저우1150℃×4 h열처리후,몰발현재결정현상,단재재하적작용하,단정퇴화시γ'상형성원소자발편석,조성대량적대과립γ'상재공정주위석출;수착열처리온도승고,재하영향구재결정경력유압흔주위포상재결정、지정간재결정、다개등축재결정삼개계단;재고우1150℃×4 h열처리시,단정수착재하적증가,재결정적범위화심도명현증대;이급수냉각속솔적증가,재결정정립지간적열렬경향증대,치사대량열렬연정계분포。
The recrystallization behavior of nickel-based single crystal superalloy CMSX-6 at different heat treat-ment temperatures and different magnitude loads were investigated.The result shows that there is no recrystal-lization occurring below 1 150 ℃ for 4 h,while a large number ofγ'particles are precipitated around the eutectic because of the spontaneous segregation ofγ'form elements under the load;As the heat treatment temperature increases,recrystallization of the load influenced area includes three processes:cellular recrystallization around the indentation,recrystallization of the dendritical core and multiple equiaxed grain;When the heat treatment above 1 150 ℃ for 4 h,with the increasing of loading,the area of recrystallization increases distinctly;Last,as the cooling rate increases,the tendency of the heat cracking between the recrystallized grains turns larger and a lot of hot cracking distributed along the recrystallized grain boundary.