功能材料
功能材料
공능재료
JOURNAL OF FUNCTIONAL MATERIALS
2014年
24期
24064-24069
,共6页
王俊勃%刘松涛%杨敏鸽%贺辛亥%付翀%丁秉钧
王俊勃%劉鬆濤%楊敏鴿%賀辛亥%付翀%丁秉鈞
왕준발%류송도%양민합%하신해%부충%정병균
化学共沉淀%Fe 掺杂%纳米 SnO2%Ag 基电接触材料%放电性能
化學共沉澱%Fe 摻雜%納米 SnO2%Ag 基電接觸材料%放電性能
화학공침정%Fe 참잡%납미 SnO2%Ag 기전접촉재료%방전성능
chemical co-precipitation%Fe-doped%nanosized tin dioxide powders%Ag-based electrical contact alloy%discharging performance
利用化学共沉淀、高能球磨技术及热压烧结等方法制备出 Fe 掺杂纳米复合 Ag-SnO2电接触合金,测定了纳米复合电接触合金密度、硬度、电阻率、耐电压强度、耐烧蚀性等基本物理性能,运用扫描电镜(SEM)对电性能测试前后组织进行观察分析。结果发现,Fe元素的加入,细化了纳米 SnO2;Fe 掺杂含量越多,纳米氧化物粒度越小,纳米复合电接触合金组织也越细小均匀,纳米复合电接触材料硬度、电阻率、平均耐电压强度和电弧寿命上升,截流值降低;且 Fe 掺杂对纳米复合电接触合金电弧烧蚀速率有明显影响。
利用化學共沉澱、高能毬磨技術及熱壓燒結等方法製備齣 Fe 摻雜納米複閤 Ag-SnO2電接觸閤金,測定瞭納米複閤電接觸閤金密度、硬度、電阻率、耐電壓彊度、耐燒蝕性等基本物理性能,運用掃描電鏡(SEM)對電性能測試前後組織進行觀察分析。結果髮現,Fe元素的加入,細化瞭納米 SnO2;Fe 摻雜含量越多,納米氧化物粒度越小,納米複閤電接觸閤金組織也越細小均勻,納米複閤電接觸材料硬度、電阻率、平均耐電壓彊度和電弧壽命上升,截流值降低;且 Fe 摻雜對納米複閤電接觸閤金電弧燒蝕速率有明顯影響。
이용화학공침정、고능구마기술급열압소결등방법제비출 Fe 참잡납미복합 Ag-SnO2전접촉합금,측정료납미복합전접촉합금밀도、경도、전조솔、내전압강도、내소식성등기본물이성능,운용소묘전경(SEM)대전성능측시전후조직진행관찰분석。결과발현,Fe원소적가입,세화료납미 SnO2;Fe 참잡함량월다,납미양화물립도월소,납미복합전접촉합금조직야월세소균균,납미복합전접촉재료경도、전조솔、평균내전압강도화전호수명상승,절류치강저;차 Fe 참잡대납미복합전접촉합금전호소식속솔유명현영향。
The Fe-doped nanocomposite Ag-SnO2 contact alloys were prepared by chemical co-precipitation method,high-energy ball milling,hot pressing and sintering technique.The density,hardness,resistivity, brakdown strength and electrical arc erosion of alloys were measured,and the microstructures of the nanocom-posite contact alloys were analyzed by field emission scanning electron microscopy (FESEM).Results show that the nanosized of SnO2 particles were refined doped with Fe,when Fe concentration increases,the size of oxide particles in nanocomposite Ag-SnO2 contact decreases further,and the microstructures of alloys are more ho-mogenous and fine.Meanwhile the hardness,resistivity,average filed strength and arcing life of nanocomposite Ag-SnO2 contact increase,but its the current chopping value decrease.While the Fe-doping concentration has obviously influence on the arc ablation rate of nanocomposite electrical contact alloys.