化工技术与开发
化工技術與開髮
화공기술여개발
TECHNOLOGY & DVELOPMENT OF CHEMICAL INDUSTRY
2014年
12期
15-17
,共3页
AuSiO2%包裹%核壳结构%Yolk/shell结构
AuSiO2%包裹%覈殼結構%Yolk/shell結構
AuSiO2%포과%핵각결구%Yolk/shell결구
AuSiO2%coat%core shell structure%Yolk/shell structure
在合成贵金属Au纳米颗粒的基础上,利用种子生长法制备Au@ZnO纳米核壳结构,以正硅酸四乙酯(TEOS)为前驱体,并利用酸刻蚀ZnO包裹层得到Au@SiO2纳米Yolk/shell结构,采用透射电子显微镜、紫外–可见分光光度仪等对样品的形貌、结构及稳定性进行了系统的表征。
在閤成貴金屬Au納米顆粒的基礎上,利用種子生長法製備Au@ZnO納米覈殼結構,以正硅痠四乙酯(TEOS)為前驅體,併利用痠刻蝕ZnO包裹層得到Au@SiO2納米Yolk/shell結構,採用透射電子顯微鏡、紫外–可見分光光度儀等對樣品的形貌、結構及穩定性進行瞭繫統的錶徵。
재합성귀금속Au납미과립적기출상,이용충자생장법제비Au@ZnO납미핵각결구,이정규산사을지(TEOS)위전구체,병이용산각식ZnO포과층득도Au@SiO2납미Yolk/shell결구,채용투사전자현미경、자외–가견분광광도의등대양품적형모、결구급은정성진행료계통적표정。
t:The Au nanoparticles with different sizes were firstly synthesized and the Au@ZnO core shell nanostructure were subsequently prepared by the seed growth method. Using Tetraethyl orthosilicate (TEOS) as precursors, and the ZnO layer were etched, finally the Au@SiO2 Yolk/shelll particles were synthesized . The morphology, structure and stability properties of the samples were investigated by TEM and UV-VIS absorption spectrometer.