现代农药
現代農藥
현대농약
MODERN AGROCHEMICALS
2014年
6期
41-43
,共3页
张月%林靖凌%吕岱竹%韩丙军
張月%林靖凌%呂岱竹%韓丙軍
장월%림정릉%려대죽%한병군
柑橘%虱螨脲%灭幼脲%氟啶脲%超高效液相色谱
柑橘%虱螨脲%滅幼脲%氟啶脲%超高效液相色譜
감귤%슬만뇨%멸유뇨%불정뇨%초고효액상색보
citrus%lufenuron%chlorbenzuron%chlorfluazuron%UPLC
建立了柑橘中虱螨脲、灭幼脲和氟啶脲同时测定的超高效液相色谱(UPLC)分析方法。试样采用QuEChERS法前处理，UPLC分析。结果表明：在0.05～0.50 mg/kg添加水平时，3种农药的回收率在82.5%～100.0%之间，相对标准差为0.3%～4.3%。方法的线性范围为0.05～1.0 mg/L，3种农药的相关系数均大于0.99，最低检测浓度均为0.05 mg/kg，能满足柑橘中3种农药残留检测的要求。
建立瞭柑橘中虱螨脲、滅幼脲和氟啶脲同時測定的超高效液相色譜(UPLC)分析方法。試樣採用QuEChERS法前處理，UPLC分析。結果錶明：在0.05～0.50 mg/kg添加水平時，3種農藥的迴收率在82.5%～100.0%之間，相對標準差為0.3%～4.3%。方法的線性範圍為0.05～1.0 mg/L，3種農藥的相關繫數均大于0.99，最低檢測濃度均為0.05 mg/kg，能滿足柑橘中3種農藥殘留檢測的要求。
건립료감귤중슬만뇨、멸유뇨화불정뇨동시측정적초고효액상색보(UPLC)분석방법。시양채용QuEChERS법전처리，UPLC분석。결과표명：재0.05～0.50 mg/kg첨가수평시，3충농약적회수솔재82.5%～100.0%지간，상대표준차위0.3%～4.3%。방법적선성범위위0.05～1.0 mg/L，3충농약적상관계수균대우0.99，최저검측농도균위0.05 mg/kg，능만족감귤중3충농약잔류검측적요구。
An UPLC method to measure the residues of lufenuron, chlorbenzuron and chlorfluazuron in citrus was established. The samples were treated by QuEChERS method, then determined by UPLC. When the spiked levels of the three pesticides were 0.05, 0.10, 0.50 mg/kg, the average recoveries were 82.5%-100.0%, and the relative standard deviations (RSD) were 0.3%-4.3% (n=5). The calibration curve was linear in the range of 0.05-1.0 mg/L, the correlation coefficients of the three pesticides were more than 0.99, the limits of quantification (LOQ) were 0.05 mg/kg.
