安徽化工
安徽化工
안휘화공
ANHUI CHEMICAL INDUSTRY
2014年
6期
36-40
,共5页
响应面法%杜鹃花%超声辅助提取%黄酮
響應麵法%杜鵑花%超聲輔助提取%黃酮
향응면법%두견화%초성보조제취%황동
Response Surface Method%Rhododendron%Ultrasound-assisted extraction%Flavonoids
利用响应面法对超声提取杜鹃花黄酮类成分的工艺条件进行优化。在对乙醇体积分数、料液比、提取时间单因子实验的基础上,根据中心组合设计原理,采用三因子三水平的响应面分析法,在分析各个因素的显著性和交互作用后,得出超声辅助提取杜鹃花黄酮的最优工艺条件:乙醇的体积分数为74.08%,料液比为20.58∶1,提取时间为32.48 min,此时黄酮平均提取率为8.758%。
利用響應麵法對超聲提取杜鵑花黃酮類成分的工藝條件進行優化。在對乙醇體積分數、料液比、提取時間單因子實驗的基礎上,根據中心組閤設計原理,採用三因子三水平的響應麵分析法,在分析各箇因素的顯著性和交互作用後,得齣超聲輔助提取杜鵑花黃酮的最優工藝條件:乙醇的體積分數為74.08%,料液比為20.58∶1,提取時間為32.48 min,此時黃酮平均提取率為8.758%。
이용향응면법대초성제취두견화황동류성분적공예조건진행우화。재대을순체적분수、료액비、제취시간단인자실험적기출상,근거중심조합설계원리,채용삼인자삼수평적향응면분석법,재분석각개인소적현저성화교호작용후,득출초성보조제취두견화황동적최우공예조건:을순적체적분수위74.08%,료액비위20.58∶1,제취시간위32.48 min,차시황동평균제취솔위8.758%。
Response Surface Method was applied to optimize the Ultrasound-assisted extraction of the total flavonoids from Rhododendron. On the basis of single factor experiments, the optimum conditions for the Ultrasound-assisted extraction of flavonoids from Rhododendron were obtained through Box-Benhnken center-united experiment design and Response Surface Method with 3 factors and 3 level. On the analysis of various factors significant and interaction, the optimum Ultrasound-assisted extraction conditions of flavonoids from Rhododendron were as follows:the ethanol content is 74.08%, the ratio of solid to liquid is 20.58∶1 and extraction time is 32.48 min.Under such condition, the average extraction rate could be up to 8.758%.