化学研究与应用
化學研究與應用
화학연구여응용
CHEMICAL RESEARCH AND APPLICATION
2014年
12期
1953-1957
,共5页
黄宏升%金华峰%马飞%郑佳%王芹芹%张宇
黃宏升%金華峰%馬飛%鄭佳%王芹芹%張宇
황굉승%금화봉%마비%정가%왕근근%장우
MgBO2(OH):Eu3+%纳米%发光材料%制备
MgBO2(OH):Eu3+%納米%髮光材料%製備
MgBO2(OH):Eu3+%납미%발광재료%제비
MgBO2( OH):Eu3+%nanometer%luminescent material%preparation
利用水热法,制备得到了纳米线组装的绒球状和纳米带聚集的絮状MgBO2(OH):Eu3+,对它们进行了EDS、XRD、IR、SEM等表征及发光性能研究。研究发现两个产品的最高激发峰和发射峰分别都位于λ=250nm和λ=615nm处,为红色发光材料;且发现绒球状 MgBO2( OH):Eu3+的峰强度明显强于絮状 MgBO2( OH):Eu3+,但絮状MgBO2( OH):Eu3+的红橙比( R/O)更高。
利用水熱法,製備得到瞭納米線組裝的絨毬狀和納米帶聚集的絮狀MgBO2(OH):Eu3+,對它們進行瞭EDS、XRD、IR、SEM等錶徵及髮光性能研究。研究髮現兩箇產品的最高激髮峰和髮射峰分彆都位于λ=250nm和λ=615nm處,為紅色髮光材料;且髮現絨毬狀 MgBO2( OH):Eu3+的峰彊度明顯彊于絮狀 MgBO2( OH):Eu3+,但絮狀MgBO2( OH):Eu3+的紅橙比( R/O)更高。
이용수열법,제비득도료납미선조장적융구상화납미대취집적서상MgBO2(OH):Eu3+,대타문진행료EDS、XRD、IR、SEM등표정급발광성능연구。연구발현량개산품적최고격발봉화발사봉분별도위우λ=250nm화λ=615nm처,위홍색발광재료;차발현융구상 MgBO2( OH):Eu3+적봉강도명현강우서상 MgBO2( OH):Eu3+,단서상MgBO2( OH):Eu3+적홍등비( R/O)경고。
The pompon-like and flocculent-like MgBO2( OH):Eu3+ which were assembled by nanosheets and nanobelts respectively were prepared by hydrothermal method. They were characterized by EDS,XRD,IR,SEM,and their luminescence properties were al-so studied. The results show that the maximum excitation peak and emission peaks of these two products were located at the λ=250nm and λ=615nm respectively,they were red luminescence material;In addition,it was found that the pompon-like MgBO2 (OH):Eu3+ show stronger peak intensity than flocculent-like MgBO2(OH):Eu3+,while flocculent-like MgBO2(OH):Eu3+show higher red to orange intensity ratio( R/O).