世界科学技术-中医药现代化
世界科學技術-中醫藥現代化
세계과학기술-중의약현대화
WORLD SCIENCE AND TECHNOLOGY-MODERNIZATION OF TRADITIONAL CHINESE MEDICINE
2014年
11期
2385-2389
,共5页
雷咪%陈龙%黄必胜%陈科力%袁明洋
雷咪%陳龍%黃必勝%陳科力%袁明洋
뢰미%진룡%황필성%진과력%원명양
近红外光谱法%多元散射校正%硫酸盐类%矿物药
近紅外光譜法%多元散射校正%硫痠鹽類%礦物藥
근홍외광보법%다원산사교정%류산염류%광물약
Near-infrared spectroscopy%hierarchical clustering method%sulfate%mineral medicine
目的:建立7种含硫酸盐的矿物类中药的近红外光谱鉴别方法。方法:通过对7种含硫酸盐的矿物类中药粉碎过筛后,测量各样品在12000-4000 cm-1区段范围内的近红外光谱,图谱信号经过不同的预处理方法,筛选不同的特征谱段后提取有效信息,采用聚类分析方法进行定性鉴别。结果:在8600-8100 cm-1、5843-4245 cm-1、7096-6337 cm-1谱段范围内,图谱信号经过矢量归一化和多元散射校正后,K-均值聚类分析法将20批次硫酸盐类矿物药分为7类,分析结果与传统性状方法鉴定结果基本一致。结论:该方法简便、快速,可用于这7种含硫酸盐的矿物类中药的定性鉴别与质量控制。
目的:建立7種含硫痠鹽的礦物類中藥的近紅外光譜鑒彆方法。方法:通過對7種含硫痠鹽的礦物類中藥粉碎過篩後,測量各樣品在12000-4000 cm-1區段範圍內的近紅外光譜,圖譜信號經過不同的預處理方法,篩選不同的特徵譜段後提取有效信息,採用聚類分析方法進行定性鑒彆。結果:在8600-8100 cm-1、5843-4245 cm-1、7096-6337 cm-1譜段範圍內,圖譜信號經過矢量歸一化和多元散射校正後,K-均值聚類分析法將20批次硫痠鹽類礦物藥分為7類,分析結果與傳統性狀方法鑒定結果基本一緻。結論:該方法簡便、快速,可用于這7種含硫痠鹽的礦物類中藥的定性鑒彆與質量控製。
목적:건립7충함류산염적광물류중약적근홍외광보감별방법。방법:통과대7충함류산염적광물류중약분쇄과사후,측량각양품재12000-4000 cm-1구단범위내적근홍외광보,도보신호경과불동적예처리방법,사선불동적특정보단후제취유효신식,채용취류분석방법진행정성감별。결과:재8600-8100 cm-1、5843-4245 cm-1、7096-6337 cm-1보단범위내,도보신호경과시량귀일화화다원산사교정후,K-균치취류분석법장20비차류산염류광물약분위7류,분석결과여전통성상방법감정결과기본일치。결론:해방법간편、쾌속,가용우저7충함류산염적광물류중약적정성감별여질량공제。
To establish seven kinds of minerals containing sulfate kind of near infrared spectral identification method <br> of traditional Chinese medicine (TCM). 7 species of mineral medicine containing sulfate after crushing sieving, measure all the samples in 12 000-4 000 cm-1 section within the scope of the near infrared spectrum, spectrum signal by different pretreatment methods, after the screening of the different characteristics of the spectrum to extract the effective information, using cluster analysis method for qualitative identification. In 8 600-8 100 cm-1, 5 843-4 245 cm-1, 7 096-6 337 cm -1 section within the scope of the atlas signal after the vector normalization and multiple scattering correction, K-average clustering analysis to 20 batches sulfate kind of mineral medicine is divided into seven categories, the results of the analysis method and the traditional traits identification results are basically identical. This method is simple, fast, and can be used for these minerals containing sulfate class the qualitative identification and quality control of Chinese traditional medicine.